Benzamide, 4-chloro-N-(2,2-dichloroethenyl)-

Base Information

Chemical Name:Benzamide, 4-chloro-N-(2,2-dichloroethenyl)-
CAS No.:54888-31-2
Molecular Formula:C9H6Cl3NO
Molecular Weight:250.512
Hs Code.:2924299090
European Community (EC) Number:654-056-1
DSSTox Substance ID:DTXSID70354901
Nikkaji Number:J1.511.369C

Synonyms:Benzamide, 4-chloro-N-(2,2-dichloroethenyl)-;54888-31-2;4-Chloro-N-(2,2-dichloro-vinyl)-benzamide;CBMicro_008981;DTXSID70354901;SMSF0003729;AKOS000521663;CB11683;BIM-0009133.P001

Suppliers and Price of Benzamide, 4-chloro-N-(2,2-dichloroethenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-CHLORO-N-(2,2-DICHLORO-VINYL)-BENZAMIDE 95.00%
5MG
$ 503.01

Total 0 raw suppliers

Chemical Property of Benzamide, 4-chloro-N-(2,2-dichloroethenyl)-

Chemical Property:

PSA：29.10000
LogP:3.73720
XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:248.951497
Heavy Atom Count:14
Complexity:230

Purity/Quality:: 4-CHLORO-N-(2,2-DICHLORO-VINYL)-BENZAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C(=O)NC=C(Cl)Cl)Cl

Technology Process of Benzamide, 4-chloro-N-(2,2-dichloroethenyl)-

There total 8 articles about Benzamide, 4-chloro-N-(2,2-dichloroethenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: acetic acid 2,2,2-trichloro-1-(4-chloro-benzoylamino)-ethyl ester

: 54888-31-2
N-(2,2-dichlorovinyl)-4-chlorobenzamide

Guidance literature:: With samarium diiodide; In tetrahydrofuran; at 20 ℃; for 0.0833333h;

Reference yield: 75.0%

: 53998-66-6
p-chlorobenzoic acid 1,2,2,2-tetrachloroethylamide

: 54888-31-2
N-(2,2-dichlorovinyl)-4-chlorobenzamide

Guidance literature:: With lithium perchlorate; In acetonitrile; at 15 ℃; Electrochemical reaction; cathode - mercury pool, anode - platinum plate, cathodic potential - 0.45 V vs SCE, electricity consumption - 2 F/mol;
DOI:10.1016/S0040-4020(01)00434-3

Reference yield:

: 56737-17-8
N-(2,2,2-trichloro-1-hydroxyethyl)-4-chlorobenzamide

: 54888-31-2
N-(2,2-dichlorovinyl)-4-chlorobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂ / 0 - 20 °C

2: 94 percent / SmI₂ / tetrahydrofuran / 0.08 h / 20 °C

With samarium diiodide; triethylamine; In tetrahydrofuran; dichloromethane;