Benzenecarboximidoyl chloride, 4-chloro-N-(2,2-dichloroethenyl)-

Base Information

• Chemical Name: Benzenecarboximidoyl chloride, 4-chloro-N-(2,2-dichloroethenyl)-
• CAS No.: 64516-54-7
• Molecular Formula: C9H5Cl4N
• Molecular Weight: 268.957
• DSSTox Substance ID: DTXSID80357064
• Mol file: 64516-54-7.mol

Synonyms:64516-54-7;Benzenecarboximidoyl chloride, 4-chloro-N-(2,2-dichloroethenyl)-;DTXSID80357064

Chemical Property of Benzenecarboximidoyl chloride, 4-chloro-N-(2,2-dichloroethenyl)-

Chemical Property:

• XLogP3: 4.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 268.914660
• Heavy Atom Count: 14
• Complexity: 237

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1C(=NC=C(Cl)Cl)Cl)Cl

Technology Process of Benzenecarboximidoyl chloride, 4-chloro-N-(2,2-dichloroethenyl)-

There total 4 articles about Benzenecarboximidoyl chloride, 4-chloro-N-(2,2-dichloroethenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

N-(2,2-dichlorovinyl)-4-chlorobenzamide (54888-31-2) → N-(2,2-dichlorovinyl)-4-chlorobenzimidoyl chloride (64516-54-7)

Guidance literature:

With phosphorus pentachloride; In toluene; at 45 ℃; for 2h;

DOI:10.1002/jhet.3558

Reference yield:

Methyl-N-(2.2-dichlorvinyl)p-chlorbenzimidat (64528-24-1) → N-(2,2-dichlorovinyl)-4-chlorobenzimidoyl chloride (64516-54-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl / dioxane

2: PCl₅

With hydrogenchloride; phosphorus pentachloride; In 1,4-dioxane;

Reference yield:

p-chlorobenzoic acid 1,2,2,2-tetrachloroethylamide (53998-66-6) → N-(2,2-dichlorovinyl)-4-chlorobenzimidoyl chloride (64516-54-7)

Guidance literature:

Multi-step reaction with 2 steps

1: Electrochemical reaction

2: phosphorus pentachloride / toluene / 2 h / 45 °C

With phosphorus pentachloride; In toluene;

DOI:10.1002/jhet.3558

upstream raw materials:

N-(2,2-dichlorovinyl)-4-chlorobenzamide

Methyl-N-(2.2-dichlorvinyl)p-chlorbenzimidat

p-chlorobenzoic acid 1,2,2,2-tetrachloroethylamide

N-(2,2,2-trichloro-1-hydroxyethyl)-4-chlorobenzamide

Downstream raw materials:

4-[4-chloro-N-(2,2-dichloro-vinyl)-benzimidoyl]-morpholine

Methyl-N-(2.2-dichlorvinyl)p-chlorbenzimidat

4-chloro-N-(2,2-dichloro-vinyl)-thiobenzamide

4-(4-Chloro-phenyl)-6-phenyl-2-trichloromethyl-1,2-dihydro-[1,3,5]triazine; hydrochloride