Benzaldehyde, 2,4-dimethoxy-6-(phenylmethoxy)-

Base Information

Chemical Name:Benzaldehyde, 2,4-dimethoxy-6-(phenylmethoxy)-
CAS No.:54917-02-1
Molecular Formula:C16H16O4
Molecular Weight:272.301
Hs Code.:
DSSTox Substance ID:DTXSID50356165
Wikidata:Q82135380

Synonyms:Benzaldehyde, 2,4-dimethoxy-6-(phenylmethoxy)-;54917-02-1;2,4-dimethoxy-6-phenylmethoxybenzaldehyde;2-(benzyloxy)-4,6-dimethoxybenzaldehyde;Oprea1_095644;DTXSID50356165;CS-0453660;AO-079/15259085

Suppliers and Price of Benzaldehyde, 2,4-dimethoxy-6-(phenylmethoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-(BENZYLOXY)-4,6-DIMETHOXYBENZALDEHYDE 95.00%
5MG
$ 495.77

Total 3 raw suppliers

Chemical Property of Benzaldehyde, 2,4-dimethoxy-6-(phenylmethoxy)-

Chemical Property:

PSA：44.76000
LogP:3.09530
XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:272.10485899
Heavy Atom Count:20
Complexity:288

Purity/Quality:

99% ^*data from raw suppliers

2-(BENZYLOXY)-4,6-DIMETHOXYBENZALDEHYDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC(=C(C(=C1)OCC2=CC=CC=C2)C=O)OC

Technology Process of Benzaldehyde, 2,4-dimethoxy-6-(phenylmethoxy)-

There total 4 articles about Benzaldehyde, 2,4-dimethoxy-6-(phenylmethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 708-76-9
2-hydroxy-4,6-dimethoxybenzaldehyde

: 100-44-7
benzyl chloride

: 54917-02-1
2-(benzyloxy)-4,6-dimethoxybenzaldehyde

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 8h;
DOI:10.1016/j.ejmech.2011.12.008

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 54917-02-1
2-(benzyloxy)-4,6-dimethoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) phosphoryl chloride; 2.) K₂CO₃ / 1.) acetonitrile, 30-35 deg C, 3 h; 2.) acetone, reflux, 3 h;

2: 63 percent / K₂CO₃ / dimethylformamide / 0.67 h / 150 - 153 °C

With potassium carbonate; trichlorophosphate; In N,N-dimethyl-formamide;

Reference yield:

: 830-79-5
2,4,6-trimethoxybenzaldehyde

: 54917-02-1
2-(benzyloxy)-4,6-dimethoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron tribromide / dichloromethane / -78 - 20 °C

1.2: Cooling with ice

2.1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 80 °C

With boron tribromide; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.12.008