Benzene, 1,1'-[(4-nitrophenyl)methylene]bis[2,4,6-trimethoxy-

Base Information

• Chemical Name: Benzene, 1,1'-[(4-nitrophenyl)methylene]bis[2,4,6-trimethoxy-
• CAS No.: 54921-80-1
• Molecular Formula: C25H27NO8
• Molecular Weight: 469.491
• Hs Code.: 2909309090
• DSSTox Substance ID: DTXSID90470218
• Nikkaji Number: J507.782F
• Mol file: 54921-80-1.mol

Synonyms:54921-80-1;Benzene, 1,1'-[(4-nitrophenyl)methylene]bis[2,4,6-trimethoxy-;DTXSID90470218

Chemical Property of Benzene, 1,1'-[(4-nitrophenyl)methylene]bis[2,4,6-trimethoxy-

Chemical Property:

• Boiling Point: 641.527oC at 760 mmHg
• Flash Point: 241.301oC
• PSA: 101.20000
• Density: 1.208g/cm3
• LogP: 5.34980
• XLogP3: 5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 9
• Exact Mass: 469.17366682
• Heavy Atom Count: 34
• Complexity: 559

Purity/Quality:

99% ^*data from raw suppliers

1,1'-[(4-NITROPHENYL)METHYLENE]-BIS-[2,4,6-TRIMETHOXY-BENZENE] 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC(=C(C(=C1)OC)C(C2=CC=C(C=C2)[N+](=O)[O-])C3=C(C=C(C=C3OC)OC)OC)OC

Technology Process of Benzene, 1,1'-[(4-nitrophenyl)methylene]bis[2,4,6-trimethoxy-

There total 6 articles about Benzene, 1,1'-[(4-nitrophenyl)methylene]bis[2,4,6-trimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1,2,3-trimethoxybenzene (621-23-8) + 4-nitrobenzaldehdye (555-16-8) → 2,2'-((4-nitrophenyl)methylene)bis(1,3,5-trimethoxybenzene) (54921-80-1)

Guidance literature:

With tin(IV) chloride; bis(1,5-cyclooctadiene)diiridium(I) dichloride; at 90 ℃; for 1h;

DOI:10.1021/jo062633n

Reference yield: 87.0%

1,2,3-trimethoxybenzene (621-23-8) + N-tosyl-4-nitrobenzaldimine (13707-46-5) → 4-methyl-N-((4-nitrophenyl)(2,4,6-trimethoxyphenyl)methyl)benzenesulfonamide (1228802-86-5) + 2,2'-((4-nitrophenyl)methylene)bis(1,3,5-trimethoxybenzene) (54921-80-1)

Guidance literature:

With iron(III) chloride hexahydrate; In dichloromethane; at 0 - 20 ℃; for 3.5h; Inert atmosphere;

DOI:10.1021/jo1010137

Reference yield: 56.0%

1,2,3-trimethoxybenzene (621-23-8) + tert-butyl carbazate (4248-19-5) + 4-nitrobenzaldehdye (555-16-8) → tert-butyl N-[(4-nitrophenyl)(2,4,6-trimethoxyphenyl)methyl]carbamate (1373935-55-7) + 2,2'-((4-nitrophenyl)methylene)bis(1,3,5-trimethoxybenzene) (54921-80-1)

Guidance literature:

With iodine; In tetrahydrofuran; at 20 ℃;

DOI:10.1016/j.tetlet.2012.03.024

upstream raw materials:

1,2,3-trimethoxybenzene

4-nitrobenzaldehdye

N-tosyl-4-nitrobenzaldimine

tert-butyl carbazate

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