2-Amino-1H-phenalen-1-one

Base Information

Chemical Name:2-Amino-1H-phenalen-1-one
CAS No.:55077-97-9
Molecular Formula:C13H9NO
Molecular Weight:195.221
Hs Code.:
ChEMBL ID:CHEMBL4160623
DSSTox Substance ID:DTXSID00515184
Nikkaji Number:J1.307.499B
Wikidata:Q82375942

Synonyms:2-AMINO-1H-PHENALEN-1-ONE;aminophenalenone;55077-97-9;CHEMBL4160623;DTXSID00515184

Suppliers and Price of 2-Amino-1H-phenalen-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 2-Amino-1H-phenalen-1-one

Chemical Property:

Melting Point:127-128 °C(Solv: ligroine (8032-32-4))
Boiling Point:410.4±45.0 °C(Predicted)
PSA：43.09000
Density:1.319±0.06 g/cm3(Predicted)
LogP:3.03600
XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:195.068413911
Heavy Atom Count:15
Complexity:321

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C3C(=C1)C=C(C(=O)C3=CC=C2)N

Technology Process of 2-Amino-1H-phenalen-1-one

There total 1 articles about 2-Amino-1H-phenalen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 548-39-0
Perinaphthenon

: 55077-97-9
2-amino-1H-phenalen-1-one

: 70402-14-1
6-amino-1H-phenalen-1-one

: 73693-20-6
5-aminophenalenone

Guidance literature:: Perinaphthenon; With sulfuric acid; nitric acid; at 0 - 20 ℃; for 3h;

With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 1h;
DOI:10.1016/j.ejmech.2017.10.032

Reference yield:

: 55077-97-9
2-amino-1H-phenalen-1-one

: 548-39-0
Perinaphthenon

Guidance literature:: With sodium hypophosphite; sulfuric acid; sodium nitrite; Yield given. Multistep reaction; 1) CH₃COOH, 20 deg. C, 10 min; 2) water, 30 min;

Reference yield:

: 55077-97-9
2-amino-1H-phenalen-1-one

: 6642-29-1
4-nitronaphthalic-1,8-anhydride

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / acetic acid / 2 h / Ambient temperature

2: 87 percent / conc. H₂SO₄, HNO₃ / 2 h / 1.) 0 to 2 deg C, 1 h, 2.) room temp., 1 h.

3: 78 percent / sodium bichromate / acetic acid / 10 h / Heating

With sodium dichromate; sulfuric acid; nitric acid; In acetic acid;