Technology Process of 1,1'-(Methyleneditellanyl)dibenzene
There total 5 articles about 1,1'-(Methyleneditellanyl)dibenzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dichloromethane;
In
tetrahydrofuran;
THF was distilled onto Te powder under N2, frozen (-196°C), PhLi syriged in, mixt. was allowed to thaw, after Te dissolution mixt. was refrozen (-196°C), CH2Cl2 added, warmed to room temp.; mixt. was hydrolyzed (satd. aq. NaCl), org. phase septd., dried, evapd. in vacuo; good yield;
DOI:10.1021/om00144a045
- Guidance literature:
-
Multi-step reaction with 2 steps
1: (i) Te, THF, Et2O, benzene, (ii) O2, H2O
2: diethyl ether
In
diethyl ether;