1,3-Dimethoxy-2-[(1E)-2-phenylethenyl]benzene

Base Information

Chemical Name:1,3-Dimethoxy-2-[(1E)-2-phenylethenyl]benzene
CAS No.:55288-33-0
Molecular Formula:C16H16O2
Molecular Weight:240.302
Hs Code.:
DSSTox Substance ID:DTXSID301254449
Nikkaji Number:J1.814.791B,J464.985K

Synonyms:SCHEMBL5497383;SCHEMBL5497385;DTXSID301254449;55288-33-0;1,3-Dimethoxy-2-[(1E)-2-phenylethenyl]benzene

Suppliers and Price of 1,3-Dimethoxy-2-[(1E)-2-phenylethenyl]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Dimethoxy-2-[(1E)-2-phenylethenyl]benzene

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:240.115029749
Heavy Atom Count:18
Complexity:244

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C(=CC=C1)OC)C=CC2=CC=CC=C2
Isomeric SMILES:COC1=C(C(=CC=C1)OC)/C=C/C2=CC=CC=C2

Technology Process of 1,3-Dimethoxy-2-[(1E)-2-phenylethenyl]benzene

There total 4 articles about 1,3-Dimethoxy-2-[(1E)-2-phenylethenyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1466-76-8
2-6-dimethoxybenzoic acid

: 55288-33-0
1-(2,6-dimethoxystyryl)benzene

Guidance literature:: With palladium(II) trifluoroacetate; 1-Adamantanecarboxylic acid; p-benzoquinone; In 1,4-dioxane; dimethyl sulfoxide; N,N-dimethyl-formamide; at 120 ℃; for 1h; optical yield given as %de; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol9007553

Reference yield: 97.0%

: 1449-46-3
benzyltriphenylphosphonium bromide

: 3392-97-0
2,6-dimethoxybenzaldehyde

: 55288-33-0
1-(2,6-dimethoxystyryl)benzene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 0.5h;
DOI:10.1248/cpb.40.1130

Reference yield:

: 1080-32-6
O,O-diethyl benzylphosphonate

: 3392-97-0
2,6-dimethoxybenzaldehyde

: 55288-33-0
1-(2,6-dimethoxystyryl)benzene

Guidance literature:: O,O-diethyl benzylphosphonate; With 18-crown-6 ether; sodium methylate; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h;

2,6-dimethoxybenzaldehyde; In N,N-dimethyl-formamide; at 20 - 120 ℃; for 6h;
DOI:10.1021/jm060630x