2-(((2-Hydroxyphenyl)imino)methyl)quinolin-8-ol

Base Information

• Chemical Name: 2-(((2-Hydroxyphenyl)imino)methyl)quinolin-8-ol
• CAS No.: 5548-72-1
• Molecular Formula: C16H12N2O2
• Molecular Weight: 264.27900
• DSSTox Substance ID: DTXSID90425223
• Nikkaji Number: J227.519H
• ChEMBL ID: CHEMBL242547
• Mol file: 5548-72-1.mol

Synonyms:5548-72-1;2-(((2-Hydroxyphenyl)imino)methyl)quinolin-8-ol;Oprea1_592254;8-Quinolinol, 2-[[(2-hydroxyphenyl)imino]methyl]-;CHEMBL242547;DTXSID90425223;2-[(E)-(2-hydroxyphenyl)iminomethyl]quinolin-8-ol;2-(N-(o-hydroxyphenyl)formimidoyl)-8-hydroxyquinoline;8-Quinolinol, 2-[(E)-[(2-hydroxyphenyl)imino]methyl]-;2-[(E)-[(2-HYDROXYPHENYL)IMINO]METHYL]QUINOLIN-8-OL

Chemical Property of 2-(((2-Hydroxyphenyl)imino)methyl)quinolin-8-ol

Chemical Property:

• PSA: 62.22000
• LogP: 1.24330
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 264.089877630
• Heavy Atom Count: 20
• Complexity: 347

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)N=CC2=NC3=C(C=CC=C3O)C=C2)O

Technology Process of 2-(((2-Hydroxyphenyl)imino)methyl)quinolin-8-ol

There total 2 articles about 2-(((2-Hydroxyphenyl)imino)methyl)quinolin-8-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2-formyl oxine (14510-06-6) + 2-amino-phenol (95-55-6) → N-(8-hydroxyl-2-quinolylmethylene)-o-aminophenol (5548-72-1)

Guidance literature:

In toluene; for 1h; Inert atmosphere; Schlenk technique; Dean-Stark; Reflux;

DOI:10.1002/ejic.201801160

Reference yield:

→ 2--8-hydroxychinolin (5548-72-1)

Guidance literature:

8-Hydroxychinolin-2-carbaldehyd, o-Aminophenol;

DOI:10.1246/bcsj.45.477

Reference yield: 84.0%

N-(8-hydroxyl-2-quinolylmethylene)-o-aminophenol (5548-72-1) + cobalt(II) diacetate tetrahydrate (6147-53-1) → C32H22CoN4O4

Guidance literature:

In methanol; for 1.5h; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1002/ejic.201801160

upstream raw materials:

2-formyl oxine

2-amino-phenol

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