Technology Process of 5-(2-Hydroxy-5-methylphenyl)-6-methyl-2-heptanone
There total 22 articles about 5-(2-Hydroxy-5-methylphenyl)-6-methyl-2-heptanone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
10% Pd/C; hydrogen;
In
ethyl acetate;
for 8h;
under 760.051 Torr;
DOI:10.1055/s-2008-1072733
- Guidance literature:
-
With
sulfuric acid; dihydrogen peroxide;
In
tetrahydrofuran;
for 12h;
Ambient temperature;
DOI:10.1016/0040-4020(94)00942-N
- Guidance literature:
-
Multi-step reaction with 6 steps
1: Mg / diethyl ether / 48 h rt, 24 h reflux
2: p-TsOH / benzene / 6 h / Heating
3: 97 percent / H2 / 10percent Pd-C / ethyl acetate / Ambient temperature
4: 37 percent / Jones reagent / acetone / 6 h
5: 87 percent / diethyl ether / 24 h rt, 24 h reflux
6: 76 percent / 35percent H2O2, concd. H2SO4 / tetrahydrofuran / 12 h / Ambient temperature
With
jones reagent; sulfuric acid; hydrogen; dihydrogen peroxide; toluene-4-sulfonic acid; magnesium;
palladium on activated charcoal;
In
tetrahydrofuran; diethyl ether; ethyl acetate; acetone; benzene;
DOI:10.1016/0040-4020(94)00942-N
