4,7,7-Trimethyl-3-oxobicyclo[2.2.1]heptane-1-carboxamide

Base Information

Chemical Name:4,7,7-Trimethyl-3-oxobicyclo[2.2.1]heptane-1-carboxamide
CAS No.:55784-68-4
Molecular Formula:C11H17NO2
Molecular Weight:195.25800
Hs Code.:2924299090
DSSTox Substance ID:DTXSID50396809
Mol file:55784-68-4.mol

Synonyms:4,7,7-TRIMETHYL-3-OXOBICYCLO[2.2.1]HEPTANE-1-CARBOXAMIDE;55784-68-4;SBB039338;Oprea1_008054;Oprea1_693590;DTXSID50396809;MFCD08753006;STL553091;AKOS000267659;AKOS016039179;BS-38027;CS-0366529

Suppliers and Price of 4,7,7-Trimethyl-3-oxobicyclo[2.2.1]heptane-1-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

ChemBridge Corporation
4,7,7-trimethyl-3-oxobicyclo[2.2.1]heptane-1-carboxamide 95%
250 mg
$ 31.00

American Custom Chemicals Corporation
4,7,7-TRIMETHYL-3-OXOBICYCLO[2.2.1]HEPTANE-1-CARBOXAMIDE 95.00%
5G
$ 1018.71

American Custom Chemicals Corporation
4,7,7-TRIMETHYL-3-OXOBICYCLO[2.2.1]HEPTANE-1-CARBOXAMIDE 95.00%
1G
$ 685.21

Total 8 raw suppliers

Chemical Property of 4,7,7-Trimethyl-3-oxobicyclo[2.2.1]heptane-1-carboxamide

Chemical Property:

Vapor Pressure:7.08E-05mmHg at 25°C
Boiling Point:343.4oC at 760 mmHg
Flash Point:161.5oC
PSA：60.16000
Density:1.161g/cm3
LogP:1.95750
XLogP3:0.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:195.125928785
Heavy Atom Count:14
Complexity:334

Purity/Quality:

98% ^*data from raw suppliers

4,7,7-trimethyl-3-oxobicyclo[2.2.1]heptane-1-carboxamide 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C2(CCC1(CC2=O)C(=O)N)C)C

Technology Process of 4,7,7-Trimethyl-3-oxobicyclo[2.2.1]heptane-1-carboxamide

There total 6 articles about 4,7,7-Trimethyl-3-oxobicyclo[2.2.1]heptane-1-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 945623-04-1
(1R)-4,7,7-trimethyl-3-oxo-norbornane-1-carboxylic acid

: 55784-68-4
(1R)-3-oxo-4.7.7-trimethyl-norbornane-carboxylic acid-(1)-amide

Guidance literature:: With thionyl chloride; anschliessend mit wss. Ammoniak erwaermen;

Reference yield:

: 55784-68-4
(1S)-3-oxo-4.7.7-trimethyl-norbornane-carboxylic acid-(1)-amide

: 129645-64-3
(1S)-3-oxo-4.7.7-trimethyl-norbornane-carboxylic acid-⁽¹⁾

Guidance literature:: With hydrogenchloride;

Reference yield:

: 38230-61-4
(+)-(1R)-3,3-dimethyl-2-methylene-1-norbornanecarboxylic acid

: 55784-68-4
(1R)-3-oxo-4.7.7-trimethyl-norbornane-carboxylic acid-(1)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: trichloroacetic acid / 60 - 70 °C / anschliessende Hydrolyse

2: aqueous sodium carbonate-solution; potassium permanganate / Reinigung ueber das Amid

3: thionyl chloride / anschliessend mit wss. Ammoniak erwaermen

With potassium permanganate; thionyl chloride; sodium carbonate; trichloroacetic acid;