1,4-Butanediol, 2-methylene-, 4-benzoate

Base Information

Chemical Name:1,4-Butanediol, 2-methylene-, 4-benzoate
CAS No.:558443-68-8
Molecular Formula:C₁₂H₁₄O₃
Molecular Weight:206.241
Hs Code.:

Synonyms:

Suppliers and Price of 1,4-Butanediol, 2-methylene-, 4-benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 1,4-Butanediol, 2-methylene-, 4-benzoate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,4-Butanediol, 2-methylene-, 4-benzoate

There total 4 articles about 1,4-Butanediol, 2-methylene-, 4-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-benzoyloxy-2-methylenebutanal

: 558443-68-8
benzoic acid 3-hydroxymethyl-but-3-enyl ester

Guidance literature:: With sodium tetrahydroborate; In ethanol; water; at 0 ℃; for 1h;
DOI:10.1039/d0cc06404a

Reference yield:

: 32651-37-9
4-benzoyloxybutan-1-ol

: 558443-68-8
benzoic acid 3-hydroxymethyl-but-3-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 3 h / 20 °C

2: N,N-dimethylammonium chloride / 1,2-dichloro-ethane / 70 °C

3: sodium tetrahydroborate / water; ethanol / 1 h / 0 °C

With sodium tetrahydroborate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; N,N-dimethylammonium chloride; In ethanol; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1039/d0cc06404a

Reference yield:

: 22927-31-7
4-oxobutyl benzoate

: 558443-68-8
benzoic acid 3-hydroxymethyl-but-3-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethylammonium chloride / 1,2-dichloro-ethane / 70 °C

2: sodium tetrahydroborate / water; ethanol / 1 h / 0 °C

With sodium tetrahydroborate; N,N-dimethylammonium chloride; In ethanol; water; 1,2-dichloro-ethane;
DOI:10.1039/d0cc06404a