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Copper, (4-methylphenyl)-

Base Information
  • Chemical Name:Copper, (4-methylphenyl)-
  • CAS No.:5588-74-9
  • Molecular Formula:C7H7Cu
  • Molecular Weight:154.679
  • Hs Code.:
Copper, (4-methylphenyl)-

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Chemical Property of Copper, (4-methylphenyl)-
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Technology Process of Copper, (4-methylphenyl)-

There total 1 articles about Copper, (4-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

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Guidance literature:
p-Tolyllithium, CuBr;
DOI:10.1016/S0022-328X(00)87685-8
Guidance literature:
In toluene; under N2, addn. of copper(I) benzoate to a yellow suspn. of 4-tolylcopper(I) in toluene, at -70°C, slowly raising the temp. to 0°C, over 5 h, pptn.; filtration, washing (the solid) with hexane (3x), drying in vac., cooling the filtrate to -30 °C, storing at this temp 2 d, pptn., filtration, washing with hexane (3x), drying in vac., elem. anal;
Guidance literature:
In toluene; under N2, addn. of 2-bromobenzoic acid to a yellow suspn. of 4-tolylcopper cooled to -70°C, slowly raising the temp. to -40°C (pptn.of an unidentifiable solid); filtration, recooling the orange filtrate to -80°C, storing 2 d (pptn.), filtration, washing with hexane (3x), drying in vac., elem. anal.;
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