Trimethyl[(2-methyl-1-phenylcyclopropyl)oxy]silane

Base Information

Chemical Name:Trimethyl[(2-methyl-1-phenylcyclopropyl)oxy]silane
CAS No.:56011-29-1
Molecular Formula:C13H20OSi
Molecular Weight:220.387
Hs Code.:
DSSTox Substance ID:DTXSID10504887
Nikkaji Number:J1.976.273D

Synonyms:56011-29-1;Trimethyl[(2-methyl-1-phenylcyclopropyl)oxy]silane;DTXSID10504887

Suppliers and Price of Trimethyl[(2-methyl-1-phenylcyclopropyl)oxy]silane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Trimethyl[(2-methyl-1-phenylcyclopropyl)oxy]silane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:220.128341792
Heavy Atom Count:15
Complexity:227

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CC1(C2=CC=CC=C2)O[Si](C)(C)C

Technology Process of Trimethyl[(2-methyl-1-phenylcyclopropyl)oxy]silane

There total 4 articles about Trimethyl[(2-methyl-1-phenylcyclopropyl)oxy]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37471-46-8
1-phenyl-1-trimethylsiloxypropene

: 14399-53-2
bis(iodomethyl)zinc

: 56011-29-1
1-Siloxy-1-phenyl-2-methylcyclopropane

Guidance literature:: bis(iodomethyl)zinc; With 1,2-dimethoxyethane; trichloroacetic acid; In hexane; dichloromethane; at -15 ℃; for 1h; Schlenk technique; Inert atmosphere;

1-phenyl-1-trimethylsiloxypropene; In hexane; dichloromethane; at -15 - 25 ℃; for 3h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c3ob40751a

Reference yield:

: 13735-81-4
1-styrenyloxytrimethylsilane

: 75-11-6
diiodomethane

: 56011-29-1
1-Siloxy-1-phenyl-2-methylcyclopropane

Guidance literature:: With diethylzinc; In hexane; dichloromethane; at 0 - 20 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.1c02824

Reference yield:

: 93-55-0
1-phenyl-propan-1-one

: 56011-29-1
1-Siloxy-1-phenyl-2-methylcyclopropane

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1 h / 0 °C

2: diethylzinc / dichloromethane; hexane / 1 h / 20 °C / Inert atmosphere

With diethylzinc; triethylamine; In hexane; dichloromethane;
DOI:10.1055/s-0040-1706088