hydrazinecarboxylic acid, 1-methyl-, methyl ester

Base Information

• Chemical Name: hydrazinecarboxylic acid, 1-methyl-, methyl ester
• CAS No.: 20628-41-5
• Molecular Formula: C3H8N2O2
• Molecular Weight: 104.109
• Hs Code.: 2928000090
• Mol file: 20628-41-5.mol

Synonyms:2-Methyl-carbazidsaeure-methylester;N-methyl-hydrazine-carboxylic acid methyl ester;methyl N-amino-N-methyl-carbamate;N-methylmethoxycarbohydrazide;N-methyl-N-methoxy-carbonylhydrazine;2-methyl-carbazic acid methyl ester;Methyl 1-methylhydrazinecarboxylate;N-Methyl-hydrazin-N-carbonsaeuremethylester;

Chemical Property of hydrazinecarboxylic acid, 1-methyl-, methyl ester

Chemical Property:

• Vapor Pressure: 8.68mmHg at 25°C
• Boiling Point: 132.9°Cat760mmHg
• Flash Point: 34.2°C
• PSA: 55.56000
• Density: 1.125g/cm³
• LogP: 0.25860

Purity/Quality:

98%min ^*data from raw suppliers

Methyl1-methylhydrazinecarboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of hydrazinecarboxylic acid, 1-methyl-, methyl ester

There total 6 articles about hydrazinecarboxylic acid, 1-methyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl chloroformate (79-22-1) + methylhydrazine (60-34-4) → methyl 1-methylhydrazine-1-carboxylate (20628-41-5)

Guidance literature:

With sodium hydroxide; In methanol; at 0 - 20 ℃; for 1h;

Reference yield:

methyl-nitro-carbamic acid methyl ester (14442-54-7) → methyl 1-methylhydrazine-1-carboxylate (20628-41-5)

Guidance literature:

With sulfuric acid; bei der elektrolytischen Reduktion an einer verzinnten Kupferkathode;

Reference yield:

methylhydrazine (60-34-4) + carbonic acid dimethyl ester (616-38-6) → methyl 1-methylhydrazine-1-carboxylate (20628-41-5)

Guidance literature:

In toluene; Heating;

DOI:10.1002/ardp.19713040912

upstream raw materials:

methyl-nitro-carbamic acid methyl ester

methylhydrazine

carbonic acid dimethyl ester

sulfuric acid

Downstream raw materials:

benzylidene-methyl-carbazic acid methyl ester

methylhydrazine

methyl N'-(5-chloro-2-{[2-(3-chloropyridin-2-yl)-5-(5-heptafluoropropyltetrazol-2-ylmethyl)-2H-pyrazole-3-carbonyl]amino}-3-methylbenzoyl)-N-methylhydrazinecarboxylate

N-Methyl-N'-[1-(3-nitro-phenyl)-meth-(Z)-ylidene]-hydrazinecarboxylic acid methyl ester