2-Methyl-6-pentadecylpiperidine

Base Information

Chemical Name:2-Methyl-6-pentadecylpiperidine
CAS No.:32778-79-3
Molecular Formula:C21H43N
Molecular Weight:309.5728
Hs Code.:
NSC Number:177345,177344
DSSTox Substance ID:DTXSID20954430
Nikkaji Number:J3.087.736E

Synonyms:2-methyl-6-pentadecylpiperidine;32778-79-3;METHYLPENTADECYLPIPERIDINE, CIS;SCHEMBL3214774;DTXSID20954430;UZFYSJNBWVQZQB-UHFFFAOYSA-N;NSC177344;NSC177345;NSC-177344;NSC-177345;METHYLPENTADECYLPIPERIDINE, TRANS;35285-28-0

Suppliers and Price of 2-Methyl-6-pentadecylpiperidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-Methyl-6-pentadecylpiperidine

Chemical Property:

Vapor Pressure:5.92E-06mmHg at 25°C
Boiling Point:379.3°Cat760mmHg
Flash Point:191.4°C
Density:0.826g/cm³
XLogP3:8.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:14
Exact Mass:309.339550376
Heavy Atom Count:22
Complexity:226

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCCCCCCCCC1CCCC(N1)C

Technology Process of 2-Methyl-6-pentadecylpiperidine

There total 4 articles about 2-Methyl-6-pentadecylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-methyl-6-pentadecylpyridine

: trans-2-methyl-6-pentadecylpiperidine

: 32778-79-3,35285-28-0,147329-28-0
cis-2-methyl-6-pentadecylpiperidine

Guidance literature:: With 10% Pt/activated carbon; hydrogen; acetic acid; In methanol; for 72h; under 3620.13 Torr; optical yield given as %de;
DOI:10.1016/j.tetasy.2012.05.005

Reference yield:

: 112-72-1
1-Tetradecanol

: trans-2-methyl-6-pentadecylpiperidine

: 32778-79-3,35285-28-0,147329-28-0
cis-2-methyl-6-pentadecylpiperidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / dichloromethane / 12 h / 0 - 25 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0 - 20 °C / Inert atmosphere

2.2: 2.5 h

3.1: 10% Pt/activated carbon; hydrogen; acetic acid / methanol / 72 h / 3620.13 Torr

With pyridine; n-butyllithium; 10% Pt/activated carbon; hydrogen; acetic acid; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1016/j.tetasy.2012.05.005

Reference yield:

: 72422-53-8
toluene-4-sulfonic acid tetradecyl ester

: trans-2-methyl-6-pentadecylpiperidine

: 32778-79-3,35285-28-0,147329-28-0
cis-2-methyl-6-pentadecylpiperidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0 - 20 °C / Inert atmosphere

1.2: 2.5 h

2.1: 10% Pt/activated carbon; hydrogen; acetic acid / methanol / 72 h / 3620.13 Torr

With n-butyllithium; 10% Pt/activated carbon; hydrogen; acetic acid; In tetrahydrofuran; methanol; hexane;
DOI:10.1016/j.tetasy.2012.05.005