Technology Process of Acetic acid (E)-3-dodecenyl ester
There total 20 articles about Acetic acid (E)-3-dodecenyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
at 5 - 20 ℃;
- Guidance literature:
-
With
dibenzo-18-crown-6; potassium acetate;
In
acetonitrile;
for 4h;
Heating;
DOI:10.1007/BF00958248
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 71 percent / ZnCl2 / CH2Cl2 / 2 h / 20 °C
2: 88 percent / TsOH*H2O / benzene / 0.33 h / Heating
3: H2 / Raney-Ni / ethanol / 4 h / 25 °C / 760 Torr
4: NaBH4 / ethanol / 3 h / 25 °C
5: 76 percent / Me3SiBr, ZnBr2 / CH2Cl2 / 0.5 h / 0 °C
6: 94 percent / AcOK, dibenzo-18-crown-6 / acetonitrile / 4 h / Heating
With
sodium tetrahydroborate; dibenzo-18-crown-6; trimethylsilyl bromide; hydrogen; potassium acetate; toluene-4-sulfonic acid; zinc(II) chloride; zinc dibromide;
nickel;
In
ethanol; dichloromethane; acetonitrile; benzene;
DOI:10.1007/BF00958248