1,3-Dioxane, 2-(3-chloropropyl)-5,5-dimethyl-2-phenyl-

Base Information

Chemical Name:1,3-Dioxane, 2-(3-chloropropyl)-5,5-dimethyl-2-phenyl-
CAS No.:56327-34-5
Molecular Formula:C15H21ClO2
Molecular Weight:268.784
Hs Code.:
DSSTox Substance ID:DTXSID20481493
Wikidata:Q82316935

Synonyms:56327-34-5;1,3-Dioxane, 2-(3-chloropropyl)-5,5-dimethyl-2-phenyl-;SCHEMBL10976001;DTXSID20481493

Suppliers and Price of 1,3-Dioxane, 2-(3-chloropropyl)-5,5-dimethyl-2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Dioxane, 2-(3-chloropropyl)-5,5-dimethyl-2-phenyl-

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:268.1230076
Heavy Atom Count:18
Complexity:249

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(COC(OC1)(CCCCl)C2=CC=CC=C2)C

Technology Process of 1,3-Dioxane, 2-(3-chloropropyl)-5,5-dimethyl-2-phenyl-

There total 1 articles about 1,3-Dioxane, 2-(3-chloropropyl)-5,5-dimethyl-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 939-52-6
4-chloro-1-phenylbutan-1-one

: 56327-34-5
(5,5-dimethyl-2-phenyl-1,3-dioxan-2-yl)propyl chloride

Guidance literature:: With toluene-4-sulfonic acid; In benzene;

Reference yield:

: 56327-34-5
(5,5-dimethyl-2-phenyl-1,3-dioxan-2-yl)propyl chloride

: 87696-97-7
3,4-dihydro-5-phenyl-2H-1,6-benzoxazocine

Guidance literature:: Multi-step reaction with 4 steps

1: 1) sodium hydride / 1.) DMF, 0.5 h, 2.) reflux

2: 92 percent / 75percent acetic acid / 24 h

3: 50 percent / ethanolic hydrochloride

4: 67 percent / p-toluenesulfonic acid / toluene / 18 h / Heating

With hydrogenchloride; sodium hydride; acetic acid; toluene-4-sulfonic acid; In toluene;
DOI:10.1021/jo00175a024

Reference yield:

: 56327-34-5
(5,5-dimethyl-2-phenyl-1,3-dioxan-2-yl)propyl chloride

: 87696-95-5
4-(o-aminophenoxy)butyrophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 1) sodium hydride / 1.) DMF, 0.5 h, 2.) reflux

2: 92 percent / 75percent acetic acid / 24 h

3: 50 percent / ethanolic hydrochloride

With hydrogenchloride; sodium hydride; acetic acid;
DOI:10.1021/jo00175a024