2,6-Dichloro-N-methylaniline

Base Information

Chemical Name:2,6-Dichloro-N-methylaniline
CAS No.:56462-00-1
Molecular Formula:C7H7Cl2N
Molecular Weight:176.045
Hs Code.:
European Community (EC) Number:832-960-9
DSSTox Substance ID:DTXSID90562162
Wikidata:Q82446201

Synonyms:2,6-Dichloro-N-methylaniline;56462-00-1;N-methyl-2,6-dichloroaniline;SCHEMBL463746;DTXSID90562162;FRJFKKCYRHRKRP-UHFFFAOYSA-N;MFCD00028479;AKOS012392271;EN300-148976;G31125

Suppliers and Price of 2,6-Dichloro-N-methylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2,6-Dichloro-N-methylaniline

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:174.9955546
Heavy Atom Count:10
Complexity:97.8

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CNC1=C(C=CC=C1Cl)Cl

Technology Process of 2,6-Dichloro-N-methylaniline

There total 4 articles about 2,6-Dichloro-N-methylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 608-31-1
2,6-Dichloroaniline

: 74-88-4
methyl iodide

: 56462-00-1
2,6-Dichloro-N-methylaniline

Guidance literature:: 2,6-Dichloroaniline; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -40 ℃;

methyl iodide; In tetrahydrofuran; hexane; Cooling;
DOI:10.1021/ja8019214

Reference yield: 79.5%

: 128672-28-6
2',6'-Dichloro-N-methyl-p-toluenesulfonanilide

: 56462-00-1
2,6-Dichloro-N-methylaniline

Guidance literature:: With sulfuric acid; In acetic acid; at 80 ℃; for 2h;
DOI:10.1248/cpb.38.597

Reference yield:

: 77167-07-8
N-(2,6-dichlorophenyl)-4-methylbenzenesulfonamide

: 56462-00-1
2,6-Dichloro-N-methylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 91.3 percent / 1N NaOH / 0.5 h / Heating

2: 79.5 percent / conc. H₂SO₄ / acetic acid / 2 h / 80 °C

With sodium hydroxide; sulfuric acid; In acetic acid;
DOI:10.1248/cpb.38.597