(E)-Bis(1-phenylethyl)diazene

Base Information

• Chemical Name: (E)-Bis(1-phenylethyl)diazene
• CAS No.: 5661-68-7
• Molecular Formula: C16H18N2
• Molecular Weight: 238.332
• DSSTox Substance ID: DTXSID20511845
• Nikkaji Number: J516.152E
• Mol file: 5661-68-7.mol

Synonyms:(E)-Bis(1-phenylethyl)diazene;5661-68-7;azobis( 1-phenylethane);SCHEMBL491729;DTXSID20511845

Chemical Property of (E)-Bis(1-phenylethyl)diazene

Chemical Property:

• XLogP3: 4.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 238.146998583
• Heavy Atom Count: 18
• Complexity: 224

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C1=CC=CC=C1)N=NC(C)C2=CC=CC=C2

Technology Process of (E)-Bis(1-phenylethyl)diazene

There total 7 articles about (E)-Bis(1-phenylethyl)diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

acetophenone oxime (613-91-2) → 1,1'-diphenylazoethane (5661-68-7)

Guidance literature:

With hydrazine; at 130 - 140 ℃; for 4h;

DOI:10.1134/S1070428010010124

Reference yield: 93.0%

(1-nitroethyl)benzene (7214-61-1) → 1,1'-diphenylazoethane (5661-68-7)

Guidance literature:

With hydrazine; at 130 - 140 ℃; for 4 - 5h;

DOI:10.1134/S1070428010010124

Reference yield:

N,N'-bis-(1-phenyl-ethyl)-hydrazine (94801-46-4) → 1,1'-diphenylazoethane (5661-68-7)

Guidance literature:

With air; auch mit milden Oxydationsmitteln;

upstream raw materials:

N,N'-bis-(1-phenyl-ethyl)-hydrazine

acetophenone

acetophenonazine

acetophenone oxime

Downstream raw materials:

1-phenyl-1-(2',2',6',6'-tetramethyl-1'-piperidinyloxy)ethane

2,3-diphenylbutane

1-Phenylethanol

acetophenone