1-[2-(Benzyloxy)-3,4-dimethoxyphenyl]ethan-1-one

Base Information

Chemical Name:1-[2-(Benzyloxy)-3,4-dimethoxyphenyl]ethan-1-one
CAS No.:56774-68-6
Molecular Formula:C17H18O4
Molecular Weight:286.328
Hs Code.:
DSSTox Substance ID:DTXSID90572004
Nikkaji Number:J1.097.018K
Wikidata:Q82460222

Synonyms:56774-68-6;1-[2-(Benzyloxy)-3,4-dimethoxyphenyl]ethan-1-one;SCHEMBL6452345;DTXSID90572004

Suppliers and Price of 1-[2-(Benzyloxy)-3,4-dimethoxyphenyl]ethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1-[2-(Benzyloxy)-3,4-dimethoxyphenyl]ethan-1-one

Chemical Property:

Melting Point:47-48.5 °C
Boiling Point:419.7±40.0 °C(Predicted)
Density:1.128±0.06 g/cm3(Predicted)
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:286.12050905
Heavy Atom Count:21
Complexity:325

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)C1=C(C(=C(C=C1)OC)OC)OCC2=CC=CC=C2

Technology Process of 1-[2-(Benzyloxy)-3,4-dimethoxyphenyl]ethan-1-one

There total 4 articles about 1-[2-(Benzyloxy)-3,4-dimethoxyphenyl]ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 5396-18-9
2'-hydroxy-3',4'-dimethoxyacetophenone

: 100-44-7
benzyl chloride

: 56774-68-6
2'-benzyloxy-3',4'-dimethoxyacetophenone

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium carbonate; In acetone; for 1h; Heating;

Reference yield:

: 13909-73-4
2',3',4'-trimethoxyacetophenone

: 56774-68-6
2'-benzyloxy-3',4'-dimethoxyacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / BCl₃ / CH₂Cl₂ / 0.25 h / 0 °C

2: 6.4 g / K₂CO₃ / acetone / Heating; overnight

With boron trichloride; potassium carbonate; In dichloromethane; acetone;
DOI:10.1002/jhet.5570180410