Mesityl oxide tosylhydrazone

Base Information

• Chemical Name: Mesityl oxide tosylhydrazone
• CAS No.: 5362-76-5
• Molecular Formula: C13H18N2O2S
• Molecular Weight: 266.364
• DSSTox Substance ID: DTXSID80968391
• Mol file: 5362-76-5.mol

Synonyms:mesityl oxide tosylhydrazone;DTXSID80968391;4-Methyl-N'-(4-methylpent-3-en-2-ylidene)benzene-1-sulfonohydrazide

Chemical Property of Mesityl oxide tosylhydrazone

Chemical Property:

• Vapor Pressure: 1.35E-07mmHg at 25°C
• Boiling Point: 390.6°Cat760mmHg
• Flash Point: 190°C
• Density: 1.11g/cm³
• XLogP3: 2.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 266.10889899
• Heavy Atom Count: 18
• Complexity: 420

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)S(=O)(=O)NN=C(C)C=C(C)C

Technology Process of Mesityl oxide tosylhydrazone

There total 2 articles about Mesityl oxide tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methyl-pent-3-en-2-one (141-79-7) + toluene-4-sulfonic acid hydrazide (1576-35-8) → mesityl oxide p-tosylhydrazone (5362-76-5)

Guidance literature:

In methanol;

DOI:10.1021/ja00906a018

Reference yield:

→ mesityl oxide p-tosylhydrazone (5362-76-5)

Guidance literature:

Mesityloxid, Tosylhydrazin ;

Reference yield: 85.0%

mesityl oxide p-tosylhydrazone (5362-76-5) → toluene-4-sulfonamide (70-55-3) + p-toluenesulfonyl chloride (98-59-9) + 4-(2-Chloro-2-methyl-propyl)-[1,2,3]thiadiazole + 5-(1-Chloro-1-methyl-ethyl)-4-methyl-[1,2,3]thiadiazole

Guidance literature:

With sulfur dichloride; In dichloromethane; at 20 ℃; for 0.5h; Product distribution; other reagents (SOCl₂, S₂Cl₂), products and time;

upstream raw materials:

4-methyl-pent-3-en-2-one

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

4-methyl-4-(toluene-4-sulfonyl)-pentan-2-one

2-Methyl-2-(p-toluolsulfonyl)-pentanon-⁽⁴⁾-p-toluolsulfonylhydrazon

toluene-4-sulfonamide

p-toluenesulfonyl chloride