Benzene, 1-(butyltelluro)-4-methyl-

Base Information

• Chemical Name: Benzene, 1-(butyltelluro)-4-methyl-
• CAS No.: 56950-02-8
• Molecular Formula: C11H16Te
• Molecular Weight: 275.848
• DSSTox Substance ID: DTXSID20442862
• Nikkaji Number: J1.295.061F
• Wikidata: Q82260414

Synonyms:Benzene, 1-(butyltelluro)-4-methyl-;56950-02-8;Butyl(4-methylphenyl) telluride;DTXSID20442862

Chemical Property of Benzene, 1-(butyltelluro)-4-methyl-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 4
• Exact Mass: 278.0314233
• Heavy Atom Count: 12
• Complexity: 104

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCC[Te]C1=CC=C(C=C1)C

Technology Process of Benzene, 1-(butyltelluro)-4-methyl-

There total 3 articles about Benzene, 1-(butyltelluro)-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

dibutyl ditelluride (77129-69-2) + 4-methylphenylboronic acid (5720-05-8) → n-butyl 4-methylphenyl telluride (56950-02-8)

Guidance literature:

With trichloroisocyanuric acid; In tetrahydrofuran; at 25 - 30 ℃; for 4h;

DOI:10.1002/adsc.202100371

Reference yield: 80.0%

1-bromo-butane (109-65-9) + bis(4-methylphenyl)ditelluride (32294-57-8) → n-butyl 4-methylphenyl telluride (56950-02-8)

Guidance literature:

bis(4-methylphenyl)ditelluride; With bis(η5-cyclopentadienyl)titanium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

1-bromo-butane; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; at 25 - 30 ℃; for 3h;

DOI:10.1080/00397910008087163

Reference yield: 69.0%

1-bromo-butane (109-65-9) + 4-methylphenyltellurium trichloride (30895-98-8) → n-butyl 4-methylphenyl telluride (56950-02-8)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; at 20 ℃; for 0.333333h;

DOI:10.1021/jo052061r

upstream raw materials:

1-bromo-butane

bis(4-methylphenyl)ditelluride

4-methylphenyltellurium trichloride

dibutyl ditelluride

Downstream raw materials:

4-methylphenyl(phenyl)methanol

1-phenyl-1-p-tolyl-ethylene

E-1-methyl-4-styryl-benzene

(4,4'-dimethyl-1,1'-biphenyl)

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