2,4-Dichloromesitylene

Base Information

• Chemical Name: 2,4-Dichloromesitylene
• CAS No.: 57386-83-1
• Molecular Formula: C9H10Cl2
• Molecular Weight: 189.084
• Hs Code.: 2903999090
• DSSTox Substance ID: DTXSID70395197
• Nikkaji Number: J406.562J
• Wikidata: Q82195126
• Mol file: 57386-83-1.mol

Synonyms:2,4-DICHLOROMESITYLENE;57386-83-1;2,4-dichloro-1,3,5-trimethylbenzene;1,3-DICHLORO MESITYLENE;SCHEMBL1003476;DTXSID70395197;AKOS006274832

Chemical Property of 2,4-Dichloromesitylene

Chemical Property:

• Melting Point: 59°C
• Refractive Index: 1.5590 (estimate)
• Boiling Point: 250.74°C (estimate)
• PSA: 0.00000
• Density: 1.2476 (estimate)
• LogP: 3.91860
• XLogP3: 4.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 188.0159557
• Heavy Atom Count: 11
• Complexity: 122

Purity/Quality:

98%min ^*data from raw suppliers

2,4-Dichloromesitylene ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C(C(=C1Cl)C)Cl)C

Technology Process of 2,4-Dichloromesitylene

There total 6 articles about 2,4-Dichloromesitylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1,3,5-trimethyl-benzene (108-67-8) → 1,3-dichloro-2,4,6-trimethylbenzene (57386-83-1)

Guidance literature:

With sodium chlorite; trichloroacetic acid; In dichloromethane; for 1h;

DOI:10.1007/s007060050309

Reference yield:

1,3,5-trimethyl-benzene (108-67-8) → 2-bromomesitylene (1667-04-5) + 1,3-dichloro-2,4,6-trimethylbenzene (57386-83-1)

Guidance literature:

With trichloroisocyanuric acid; at 50 - 52 ℃; for 20h; Title compound not separated from byproducts.;

DOI:10.1071/CH07261

Reference yield:

1,3,5-trimethyl-benzene (108-67-8) → 1,3,5-trichloro-2,4,6-trimethylbenzene (5324-68-5) + 2-bromomesitylene (1667-04-5) + 1,3-dichloro-2,4,6-trimethylbenzene (57386-83-1)

Guidance literature:

With Oxone; quartz; sodium chloride; In n-heptane; for 0.333333h; Milling;

DOI:10.1039/c2gc16508b

upstream raw materials:

2-bromomesitylene

1,3,5-trimethyl-benzene

chlorine

Downstream raw materials:

3,5-Dichloro-2,4,6-trimethylbenzylchlorid

mesytaldehyde

2,4,6-trimethylisophthalic dialdehyde

ethyl (3-chloro-2,4,6-trimethylphenyl)-2-oxoacetate