Ethyl mesitylglyoxylate

Base Information

Chemical Name:Ethyl mesitylglyoxylate
CAS No.:5524-57-2
Molecular Formula:C13H16O3
Molecular Weight:220.268
Hs Code.:2918300090
DSSTox Substance ID:DTXSID90371392
Nikkaji Number:J2.569.467H
Wikidata:Q82158707
Mol file:5524-57-2.mol

Synonyms:ETHYL MESITYLGLYOXYLATE;5524-57-2;ethyl 2-mesityl-2-oxoacetate;ethyl 2-oxo-2-(2,4,6-trimethylphenyl)acetate;Oxo-(2,4,6-trimethylphenyl)acetic acid ethyl ester;ETHYLMESITYLGLYOXYLATE;ethyl2-mesityl-2-oxoacetate;SCHEMBL7523545;DTXSID90371392;XRSPPFOBPRPYLD-UHFFFAOYSA-N;Ethyl mesitylglyoxylate, AldrichCPR;MFCD00151821;AKOS009157545;AS-59614;Ethyl 2-(2,4,6-trimethylphenyl)glyoxylate;CS-0206335;Ethyl 2,4,6-trimethyl-|A-oxobenzeneacetate;FT-0626201;A899767;alpha-Oxo-2,4,6-trimethylbenzeneacetic acid ethyl ester;Ethyl (2,4,6-trimethylphenyl)glyoxylate~Mesitylglyoxylic acid ethyl ester

Suppliers and Price of Ethyl mesitylglyoxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Rieke Metals
Oxo-(2,4,6-trimethylphenyl)aceticacidethylester
1g
$ 394.00

Rieke Metals
Oxo-(2,4,6-trimethylphenyl)aceticacidethylester
5g
$ 794.00

Atlantic Research Chemicals
EthylMesitylglyoxylate 95%
1gm:
$ 31.81

American Custom Chemicals Corporation
ETHYL-2-(2,4,6-TRIMETHYLPHENYL)GLYOXYLATE 95.00%
250MG
$ 652.46

Alfa Aesar
Ethyl mesitylglyoxylate, 97%
25g
$ 130.00

Alfa Aesar
Ethyl mesitylglyoxylate, 97%
5g
$ 40.50

Total 9 raw suppliers

Chemical Property of Ethyl mesitylglyoxylate

Chemical Property:

Vapor Pressure:8.14E-05mmHg at 25°C
Refractive Index:1.51
Boiling Point:341.3°Cat760mmHg
Flash Point:154.4°C
PSA：43.37000
Density:1.067g/cm³
LogP:2.35760
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:220.109944368
Heavy Atom Count:16
Complexity:260

Purity/Quality:

97% ^*data from raw suppliers

Oxo-(2,4,6-trimethylphenyl)aceticacidethylester ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi,Xn
Statements: 22
Safety Statements: 24/25

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(=O)C1=C(C=C(C=C1C)C)C

Technology Process of Ethyl mesitylglyoxylate

There total 10 articles about Ethyl mesitylglyoxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1667-04-5
2-bromomesitylene

: 4755-77-5
Ethyl oxalyl chloride

: 5524-57-2
ethyl 2-(2,4,6-trimethylphenyl)-2-oxoacetate

Guidance literature:: 2-bromomesitylene; With lithium; In diethyl ether; at 20 ℃; for 3h;

With copper(l) cyanide; In tetrahydrofuran; diethyl ether; at -65 - -60 ℃; for 1.5h; Cooling with acetone-dry ice;

Ethyl oxalyl chloride; In tetrahydrofuran; diethyl ether; at -60 - 20 ℃;
DOI:10.1021/ol302672n

Reference yield: 60.0%

: 5524-57-2
ethyl 2-(2,4,6-trimethylphenyl)-2-oxoacetate

Guidance literature:

Reference yield: 56.0%

: 57386-83-1
1,3-dichloro-2,4,6-trimethylbenzene

: 4755-77-5
Ethyl oxalyl chloride

: 1407160-10-4
C₁₇H₂₀O₆

: 5524-57-2
ethyl 2-(2,4,6-trimethylphenyl)-2-oxoacetate

Guidance literature:: 1,3-dichloro-2,4,6-trimethylbenzene; With naphthalene; lithium; In diethyl ether; at 20 ℃; for 24h;

Ethyl oxalyl chloride; In diethyl ether; at 20 ℃; Cooling with liquid nitrogen;
DOI:10.1021/ol302672n