2,4,6-Nonatrienoic acid, 9-(4-methoxy-2,3,6-trimethylphenyl)-3,7-dimethyl-, (E,E,E)-

Base Information

• Chemical Name: 2,4,6-Nonatrienoic acid, 9-(4-methoxy-2,3,6-trimethylphenyl)-3,7-dimethyl-, (E,E,E)-
• CAS No.: 57399-31-2
• Molecular Formula: C21H28O3
• Molecular Weight: 328.452
• Mol file: 57399-31-2.mol

Synonyms:

Chemical Property of 2,4,6-Nonatrienoic acid, 9-(4-methoxy-2,3,6-trimethylphenyl)-3,7-dimethyl-, (E,E,E)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4,6-Nonatrienoic acid, 9-(4-methoxy-2,3,6-trimethylphenyl)-3,7-dimethyl-, (E,E,E)-

There total 5 articles about 2,4,6-Nonatrienoic acid, 9-(4-methoxy-2,3,6-trimethylphenyl)-3,7-dimethyl-, (E,E,E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(4'-methoxy-2',3',6'-trimethylphenyl)-but-3-ene-2-one (54757-47-0) → trans-9-(4-Methoxy-2,3,6-trimethylphenyl)-3,7-dimethyl-2,4,6-nonatriensaeure (57399-31-2)

Guidance literature:

Multi-step reaction with 5 steps

1: H₂ / Raney-Ni

2: (i) NaH, (ii) /BRN= 2112698/

3: Na2(OCH₂CH₂OMe)2>

4: MnO₂

5: (i) NaH, (ii) /BRN= 2462624/, (iii) KOH

With manganese(IV) oxide; hydrogen; sodium bis(2-methoxyethoxy)aluminium dihydride; nickel;

DOI:10.1021/jm00217a011

Reference yield:

4-(4-methoxy-2,3,6-trimethylphenyl)butan-2-one (57399-32-3) → trans-9-(4-Methoxy-2,3,6-trimethylphenyl)-3,7-dimethyl-2,4,6-nonatriensaeure (57399-31-2)

Guidance literature:

Multi-step reaction with 4 steps

1: (i) NaH, (ii) /BRN= 2112698/

2: Na2(OCH₂CH₂OMe)2>

3: MnO₂

4: (i) NaH, (ii) /BRN= 2462624/, (iii) KOH

With manganese(IV) oxide; sodium bis(2-methoxyethoxy)aluminium dihydride;

DOI:10.1021/jm00217a011

Reference yield:

trans-5-(4-Methoxy-2,3,6-trimethylphenyl)-3-methyl-2-penten-1-ol (57399-34-5) → trans-9-(4-Methoxy-2,3,6-trimethylphenyl)-3,7-dimethyl-2,4,6-nonatriensaeure (57399-31-2)

Guidance literature:

Multi-step reaction with 2 steps

1: MnO₂

2: (i) NaH, (ii) /BRN= 2462624/, (iii) KOH

With manganese(IV) oxide;

DOI:10.1021/jm00217a011

upstream raw materials:

4-(4-methoxy-2,3,6-trimethylphenyl)butan-2-one

trans-5-(4-Methoxy-2,3,6-trimethylphenyl)-3-methyl-2-penten-1-ol

trans-5-(4-Methoxy-2,3,6-trimethylphenyl)-3-methyl-2-pentensaeureethylester

4-(4'-methoxy-2',3',6'-trimethylphenyl)-but-3-ene-2-one