Benzenemethanol, a-octyl-

Base Information

• Chemical Name: Benzenemethanol, a-octyl-
• CAS No.: 57716-72-0
• Molecular Formula: C₁₅H₂₄O
• Molecular Weight: 220.355
• Mol file: 57716-72-0.mol

Synonyms:1-phenylnonan-1-ol;1-phenyl-nonan-1-ol;(+/-)-1-Hydroxy-1-phenyl-nonan;

Chemical Property of Benzenemethanol, a-octyl-

Chemical Property:

• PSA: 20.23000
• LogP: 4.47060

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenemethanol, a-octyl-

There total 26 articles about Benzenemethanol, a-octyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4,4,5,5-tetramethyl-2-octyl-[1,3,2]dioxaborolane (66217-56-9) + benzaldehyde (100-52-7) → 1-phenylnonan-1-ol (57716-72-0,92660-98-5,131320-85-9,131320-86-0)

Guidance literature:

4,4,5,5-tetramethyl-2-octyl-[1,3,2]dioxaborolane; With tetramethylenebis(magnesium chloride); In tetrahydrofuran; toluene; at 0 - 20 ℃; for 1h; Inert atmosphere;

benzaldehyde; In tetrahydrofuran; toluene; at -78 ℃; for 5h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; toluene;

DOI:10.1002/anie.201201704

Reference yield: 88.0%

benzaldehyde (100-52-7) → 1-phenylnonan-1-ol (57716-72-0,92660-98-5,131320-85-9,131320-86-0)

Guidance literature:

With zinc dibromide; In tetrahydrofuran; at 25 ℃; for 3h;

DOI:10.1021/jo00116a007

Reference yield: 84.0%

1-bromo-octane (111-83-1) + benzaldehyde (100-52-7) → 1-phenylnonan-1-ol (57716-72-0,92660-98-5,131320-85-9,131320-86-0)

Guidance literature:

1-bromo-octane; With magnesium; In diethyl ether; ethylene dibromide; at 20 ℃; for 1h;

benzaldehyde; In diethyl ether; ethylene dibromide;

DOI:10.1055/s-0035-1560549

upstream raw materials:

nonan-1-al

iodobenzene

1-bromo-octane

benzaldehyde

Downstream raw materials:

1-phenylnonan-1-one

1-Brom-1-phenyl-nonan