Technology Process of 6-[(4-phenyl-1,3-thiazol-2-yl)sulfonyl]quinazoline-2,4-diamine
There total 5 articles about 6-[(4-phenyl-1,3-thiazol-2-yl)sulfonyl]quinazoline-2,4-diamine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide; acetic acid;
for 48h;
Ambient temperature;
DOI:10.1002/jhet.5570170127
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 40 percent / K2CO3 / acetone / 20 h / Ambient temperature
2: 66 percent / SnCl2*2H2O, conc. HCl / acetic acid / 18 h / Ambient temperature
3: 48 percent / various solvent(s) / 0.33 h / 160 °C
4: 63 percent / 30percent H2O2, acetic acid / 48 h / Ambient temperature
With
hydrogenchloride; dihydrogen peroxide; potassium carbonate; acetic acid; tin(ll) chloride;
In
acetic acid; acetone;
DOI:10.1002/jhet.5570170127
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 40 percent / K2CO3 / acetone / 20 h / Ambient temperature
2: 66 percent / SnCl2*2H2O, conc. HCl / acetic acid / 18 h / Ambient temperature
3: 48 percent / various solvent(s) / 0.33 h / 160 °C
4: 63 percent / 30percent H2O2, acetic acid / 48 h / Ambient temperature
With
hydrogenchloride; dihydrogen peroxide; potassium carbonate; acetic acid; tin(ll) chloride;
In
acetic acid; acetone;
DOI:10.1002/jhet.5570170127