2-(trimethylsilyl)prop-2-enal

Base Information

Chemical Name:2-(trimethylsilyl)prop-2-enal
CAS No.:58107-33-8
Molecular Formula:C6H12OSi
Molecular Weight:
Hs Code.:
DSSTox Substance ID:DTXSID20447099
Nikkaji Number:J573.009K
Wikidata:Q82265891

Synonyms:2-Trimethylsilylpropenal;58107-33-8;2-(Trimethylsilyl)acrylaldehyde;2-Propenal, 2-(trimethylsilyl)-;2-trimethylsilylprop-2-enal;starbld0003392;2-(Trimethylsilyl)propenal;DTXSID20447099;AKOS006333245;FT-0685788;J-510359

Suppliers and Price of 2-(trimethylsilyl)prop-2-enal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-(trimethylsilyl)prop-2-enal

Chemical Property:

Vapor Pressure:4.47mmHg at 25°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:128.065741536
Heavy Atom Count:8
Complexity:110

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C)C(=C)C=O

Technology Process of 2-(trimethylsilyl)prop-2-enal

There total 5 articles about 2-(trimethylsilyl)prop-2-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 55287-89-3
2-(trimethylsilyl)prop-2-en-1-ol

: 58107-33-8
2-(trimethylsilyl)acrylaldehyde

Guidance literature:: With jones reagent; In acetone; for 3h;
DOI:10.1080/00397919408013817

Reference yield:

: 13683-41-5
1-bromo-1-(trimethylsilyl)ethene

: 58107-33-8
2-(trimethylsilyl)acrylaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg, I₂, 2.) 2,2'-bipyridyl / 1.) THF, reflux, 2.5 h, 2.) THF, from 50 deg C to 55 deg C, 5 h

2: 60 percent / Jones reagent / acetone / 3 h

With [2,2]bipyridinyl; jones reagent; iodine; magnesium; In acetone;
DOI:10.1080/00397919408013817