2H-Azirine, 2-(3-butenyl)-2-methyl-3-phenyl-

Base Information

Chemical Name:2H-Azirine, 2-(3-butenyl)-2-methyl-3-phenyl-
CAS No.:58130-08-8
Molecular Formula:C13H15N
Molecular Weight:185.269
Hs Code.:
DSSTox Substance ID:DTXSID50481587

Synonyms:58130-08-8;2-(But-3-en-1-yl)-2-methyl-3-phenyl-2H-azirine;2H-Azirine, 2-(3-butenyl)-2-methyl-3-phenyl-;DTXSID50481587

Suppliers and Price of 2H-Azirine, 2-(3-butenyl)-2-methyl-3-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2H-Azirine, 2-(3-butenyl)-2-methyl-3-phenyl-

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:185.120449483
Heavy Atom Count:14
Complexity:248

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C(=N1)C2=CC=CC=C2)CCC=C

Technology Process of 2H-Azirine, 2-(3-butenyl)-2-methyl-3-phenyl-

There total 5 articles about 2H-Azirine, 2-(3-butenyl)-2-methyl-3-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 107112-66-3
iodure d'N,N,N-trimethylhydrazonium de methyl-2 phenyl-1 hexene-5 one

: 58130-08-8
(butene-3'yl)-2 methyl-2 phenyl-3 2H-azirine

Guidance literature:: With sodium hydride; In isopropyl alcohol; for 15h; Ambient temperature;

Reference yield:

: 19679-59-5
propiophenone N,N-dimethylhydrazone

: 58130-08-8
(butene-3'yl)-2 methyl-2 phenyl-3 2H-azirine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.5 M n-butyllithium / tetrahydrofuran; hexane

2: 98 percent / 36 h

3: 51 percent / sodium hydride / propan-2-ol / 15 h / Ambient temperature

With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane; isopropyl alcohol;

Reference yield:

: 58130-12-4
N,N-dimethylhydrazone de methyl-2 phenyl-1 hexene-5 one

: 58130-08-8
(butene-3'yl)-2 methyl-2 phenyl-3 2H-azirine

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / 36 h

2: 51 percent / sodium hydride / propan-2-ol / 15 h / Ambient temperature

With sodium hydride; In isopropyl alcohol;