5-(3-Nitrophenyl)furan-2-carbonitrile

Base Information

Chemical Name:5-(3-Nitrophenyl)furan-2-carbonitrile
CAS No.:58158-94-4
Molecular Formula:C₁₁H₆N₂O₃
Molecular Weight:214.18
Hs Code.:
DSSTox Substance ID:DTXSID20384738
Wikidata:Q82177070

Synonyms:5-(3-Nitro-phenyl)-furan-2-carbonitrile;5-(3-nitrophenyl)furan-2-carbonitrile;58158-94-4;2-Furancarbonitrile, 5-(3-nitrophenyl)-;DTXSID20384738;CCG-50564;AKOS000299696;BB 0245898;SR-01000639932-1

Suppliers and Price of 5-(3-Nitrophenyl)furan-2-carbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 5-(3-Nitrophenyl)furan-2-carbonitrile

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:214.03784206
Heavy Atom Count:16
Complexity:317

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)[N+](=O)[O-])C2=CC=C(O2)C#N

Technology Process of 5-(3-Nitrophenyl)furan-2-carbonitrile

There total 4 articles about 5-(3-Nitrophenyl)furan-2-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-01-1
furfural

: 58158-94-4
5-(3-nitro-phenyl)-furan-2-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaNO₂, conc. HCl; 2.) CuCl₂*2H₂O / 1.) water, 0.5 h, 0 to 5 deg C; 2.) acetone, 0 deg C

2: NH₂OH*HCl, NaOAc / ethanol; H₂O / 3.5 h / Heating

3: Ac₂O / 2.5 h / Heating

With hydrogenchloride; hydroxylamine hydrochloride; sodium acetate; acetic anhydride; sodium nitrite; In ethanol; water;

Reference yield:

: 13148-43-1
5-(3-nitrophenyl)furfural

: 58158-94-4
5-(3-nitro-phenyl)-furan-2-carbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: NH₂OH*HCl, NaOAc / ethanol; H₂O / 3.5 h / Heating

2: Ac₂O / 2.5 h / Heating

With hydroxylamine hydrochloride; sodium acetate; acetic anhydride; In ethanol; water;

Reference yield:

: 99-09-2
3-nitro-aniline

: 58158-94-4
5-(3-nitro-phenyl)-furan-2-carbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaNO₂, conc. HCl; 2.) CuCl₂*2H₂O / 1.) water, 0.5 h, 0 to 5 deg C; 2.) acetone, 0 deg C

2: NH₂OH*HCl, NaOAc / ethanol; H₂O / 3.5 h / Heating

3: Ac₂O / 2.5 h / Heating

With hydrogenchloride; hydroxylamine hydrochloride; sodium acetate; acetic anhydride; sodium nitrite; In ethanol; water;