Diethyl 5-amino-3-(2-ethoxy-2-oxoethyl)-thiophene-2,4-dicarboxylate

Base Information

Chemical Name:Diethyl 5-amino-3-(2-ethoxy-2-oxoethyl)-thiophene-2,4-dicarboxylate
CAS No.:58168-14-2
Molecular Formula:C14H19NO6S
Molecular Weight:329.36900
Hs Code.:2934999090
Mol file:58168-14-2.mol

Synonyms:5-Amino-3-ethoxycarbonylmethyl-thiophene-2,4-dicarboxylic acid diethyl ester;ethyl 2-amino-3,5-dicarbethoxythiophene-4-acetate;

Suppliers and Price of Diethyl 5-amino-3-(2-ethoxy-2-oxoethyl)-thiophene-2,4-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
Diethyl 5-amino-3-(2-ethoxy-2-oxoethyl)thiophene-2,4-dicarboxylate
1 g
$ 248.00

Matrix Scientific
Diethyl 5-amino-3-(2-ethoxy-2-oxoethyl)-thiophene-2,4-dicarboxylate
1g
$ 357.00

Total 3 raw suppliers

Chemical Property of Diethyl 5-amino-3-(2-ethoxy-2-oxoethyl)-thiophene-2,4-dicarboxylate

Chemical Property:

PSA：133.16000
LogP:2.37050

Purity/Quality:

99%, ^*data from raw suppliers

Diethyl 5-amino-3-(2-ethoxy-2-oxoethyl)thiophene-2,4-dicarboxylate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Diethyl 5-amino-3-(2-ethoxy-2-oxoethyl)-thiophene-2,4-dicarboxylate

There total 1 articles about Diethyl 5-amino-3-(2-ethoxy-2-oxoethyl)-thiophene-2,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 105-56-6
ethyl 2-cyanoacetate

: 105-50-0
diethyl 1,3-acetonedicarboxylate

: 58168-14-2
ethyl 2-amino-3,5-dicarbethoxythiophene-4-acetate

Guidance literature:: With sulfur; diethylamine; In ethanol; at 40 - 50 ℃; for 2h;
DOI:10.1246/bcsj.64.3768

Reference yield:

: 58168-14-2
ethyl 2-amino-3,5-dicarbethoxythiophene-4-acetate

: 1555-66-4
N,N-bis(2-cyanoethyl)aniline

: 139136-80-4
ethyl 5-<4-phenylazo>-2,4-bis(ethoxycarbonyl)-3-thiopheneacetate

Guidance literature:: With nitrosylsulfuric acid; acetic acid; Yield given. Multistep reaction; 1.) 0 deg C, 1 h, 2.) 0 deg C, 4 h;
DOI:10.1246/bcsj.64.3768

Reference yield:

: 58168-14-2
ethyl 2-amino-3,5-dicarbethoxythiophene-4-acetate

: 92-00-2
m-chloro-N,N-bis-β-hydroxyethylaniline

: 139174-95-1
ethyl 5-<2-chloro-4-phenylazo>-2,4-bis(ethoxycarbonyl)-3-thiopheneacetate

Guidance literature:: With nitrosylsulfuric acid; acetic acid; Yield given. Multistep reaction; 1.) 0 deg C, 1 h, 2.) 0 deg C, 4 h;
DOI:10.1246/bcsj.64.3768