Technology Process of N-phenylpropanethioamide
There total 15 articles about N-phenylpropanethioamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
propiophenone oxime;
With
triethylamine; p-toluenesulfonyl chloride;
In
acetonitrile;
at 0 - 20 ℃;
Inert atmosphere;
With
thiourea;
In
acetonitrile;
for 2h;
Reflux;
Inert atmosphere;
DOI:10.1055/s-0030-1259720
- Guidance literature:
-
With
Lawessons reagent;
In
toluene;
at 100 - 110 ℃;
for 4.33333h;
Inert atmosphere;
DOI:10.1021/acs.joc.1c00801
- Guidance literature:
-
Erhitzen auf Temoeraturen oberhalb des Schmelzpunkts;
DOI:10.1021/ja01336a032
