3,7-DIBUTYL-3,7-DIAZABICYCLO[3.3.1]NONANE

Base Information

• Chemical Name: 3,7-DIBUTYL-3,7-DIAZABICYCLO[3.3.1]NONANE
• CAS No.: 58324-90-6
• Molecular Formula: C15H30N2
• Molecular Weight: 238.41200
• Mol file: 58324-90-6.mol

Synonyms:3,7-dibutyl-3,7-diazabicyclo<3.3.1>nonane;N,N-dibutylbispidine;dibutylbispidine;3,7-dibutyl-3,7-diaza-bicyclo[3.3.1]nonane;3,7-dibutyl-3,7-diazabicyclo[3.3.1]nonane;

Chemical Property of 3,7-DIBUTYL-3,7-DIAZABICYCLO[3.3.1]NONANE

Chemical Property:

• Boiling Point: 105°/0.3mm
• PSA: 6.48000
• LogP: 2.71610

Purity/Quality:

98%min ^*data from raw suppliers

(1s,5s)-3,7-Dibutyl-3,7-diazabicyclo[3.3.1]nonane >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,7-DIBUTYL-3,7-DIAZABICYCLO[3.3.1]NONANE

There total 7 articles about 3,7-DIBUTYL-3,7-DIAZABICYCLO[3.3.1]NONANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,7-dibenzyl-9,9-(1,3-dithiolan-2-yl)-3,7-diazabicyclo[3.3.1]nonane (909037-16-7) + butan-1-ol (71-36-3) → 3,7-dibutyl-7-aza-3-azoniabicyclo[3.3.1]nonane (58324-90-6)

Guidance literature:

With nickel; at 160 ℃; for 1.5h; under 2250.18 - 13501.1 Torr; microwave irradiation;

DOI:10.1055/s-2006-942394

Reference yield:

1-Methyl-4-piperidone (1445-73-4) → 3,7-dibutyl-7-aza-3-azoniabicyclo[3.3.1]nonane (58324-90-6)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / H₂O / 1.5 h / Heating

2: 1.) AcOH, 2.) N₂H₄, KOtBu / 1.) EtOH, reflux, 7 h, 2.) BuOH, 180 deg C, 12 h

With potassium tert-butylate; potassium carbonate; acetic acid; hydrazine; In water;

DOI:10.1021/jo9708856

Reference yield:

(3,7-dibutyl-3,7-diaza-bicyclo[3.3.1]non-9-ylidene)-hydrazine → 3,7-dibutyl-7-aza-3-azoniabicyclo[3.3.1]nonane (58324-90-6)

Guidance literature:

With potassium hydroxide; at 90 ℃; for 12h;

DOI:10.1039/b309717j

upstream raw materials:

1-n-butyl-4-piperidone

N-butylamine

3,7-dibenzyl-9,9-(1,3-dithiolan-2-yl)-3,7-diazabicyclo[3.3.1]nonane

butan-1-ol

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