2-(2-Bromoethyl)-2-phenyl-1,3-dioxolane

Base Information

Chemical Name:2-(2-Bromoethyl)-2-phenyl-1,3-dioxolane
CAS No.:58521-76-9
Molecular Formula:C11H13BrO2
Molecular Weight:257.127
Hs Code.:
DSSTox Substance ID:DTXSID60548791
Wikidata:Q82427623

Synonyms:2-(2-Bromoethyl)-2-phenyl-1,3-dioxolane;58521-76-9;SCHEMBL7390254;DTXSID60548791;ZMAUGEHTQDGMRO-UHFFFAOYSA-N;2-bromoethyl-2-phenyl 1,3-dioxolane;3,3-ethylenedioxy-3-phenylpropyl bromide

Suppliers and Price of 2-(2-Bromoethyl)-2-phenyl-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of 2-(2-Bromoethyl)-2-phenyl-1,3-dioxolane

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:256.00989
Heavy Atom Count:14
Complexity:172

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COC(O1)(CCBr)C2=CC=CC=C2

Technology Process of 2-(2-Bromoethyl)-2-phenyl-1,3-dioxolane

There total 5 articles about 2-(2-Bromoethyl)-2-phenyl-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 29636-75-7
3-bromo-1-phenylpropan-1-one

: 107-21-1
ethylene glycol

: 58521-76-9
2-(2-bromoethyl)-2-phenyl-[1,3]dioxolane

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 70h; Heating;
DOI:10.1016/j.bmc.2004.02.036

Reference yield:

: 29636-75-7
3-bromo-1-phenylpropan-1-one

: 58521-76-9
2-(2-bromoethyl)-2-phenyl-[1,3]dioxolane

Guidance literature:: With toluene-4-sulfonic acid; In ethylene glycol; benzene;

Reference yield:

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 58521-76-9
2-(2-bromoethyl)-2-phenyl-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃ / CH₂Cl₂ / 5 - 25 °C

2: 50 percent / p-TsOH / benzene / 70 h / Heating

With aluminium trichloride; toluene-4-sulfonic acid; In dichloromethane; benzene; 1: Friedel-Crafts acylation;
DOI:10.1016/j.bmc.2004.02.036