N,N-Dimethyl-2-[(E)-(phenylimino)methyl]aniline

Base Information

• Chemical Name: N,N-Dimethyl-2-[(E)-(phenylimino)methyl]aniline
• CAS No.: 58758-12-6
• Molecular Formula: C15H16N2
• Molecular Weight: 224.305
• DSSTox Substance ID: DTXSID10489504

Synonyms:58758-12-6;N,N-Dimethyl-2-[(E)-(phenylimino)methyl]aniline;SCHEMBL8773391;DTXSID10489504

Chemical Property of N,N-Dimethyl-2-[(E)-(phenylimino)methyl]aniline

Chemical Property:

• XLogP3: 3.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 224.131348519
• Heavy Atom Count: 17
• Complexity: 241

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=CC=CC=C1C=NC2=CC=CC=C2

Technology Process of N,N-Dimethyl-2-[(E)-(phenylimino)methyl]aniline

There total 1 articles about N,N-Dimethyl-2-[(E)-(phenylimino)methyl]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(dimethylamino)benzaldehyde (579-72-6) + aniline (62-53-3) → ortho-C6H4(NMe2)CH=NC6H5 (58758-12-6)

Guidance literature:

With toluene-4-sulfonic acid;

Reference yield: 30.0%

5-methyl-3-phenylisoxazole (1008-74-8) + ortho-C6H4(NMe2)CH=NC6H5 (58758-12-6) → Dimethyl-{4-[(E)-2-(3-phenyl-isoxazol-5-yl)-vinyl]-phenyl}-amine (139193-97-8)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; at 60 - 70 ℃; for 4h;

DOI:10.1007/BF00778974

Reference yield: 28.0%

3,5-dimethyl-1,2-oxazole (300-87-8) + ortho-C6H4(NMe2)CH=NC6H5 (58758-12-6) → Dimethyl-{4-[(E)-2-(3-methyl-isoxazol-5-yl)-vinyl]-phenyl}-amine

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; at 60 - 70 ℃; for 4h;

DOI:10.1007/BF00778974

upstream raw materials:

2-(dimethylamino)benzaldehyde

aniline

Downstream raw materials:

Dimethyl-{4-[(E)-2-(3-phenyl-isoxazol-5-yl)-vinyl]-phenyl}-amine

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