3-methyl-6-(N-methylanilino)-5-nitro-1H-pyrimidine-2,4-dione

Base Information

Chemical Name:3-methyl-6-(N-methylanilino)-5-nitro-1H-pyrimidine-2,4-dione
CAS No.:58758-67-1
Molecular Formula:C12H12N4O4
Molecular Weight:276.252
Hs Code.:
DSSTox Substance ID:DTXSID10482257
Wikidata:Q82318398

Synonyms:58758-67-1;3-Methyl-6-(methyl(phenyl)amino)-5-nitropyrimidine-2,4(1H,3H)-dione;CTK1E8963;DTXSID10482257

Suppliers and Price of 3-methyl-6-(N-methylanilino)-5-nitro-1H-pyrimidine-2,4-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methyl-6-(N-methylanilino)-5-nitro-1H-pyrimidine-2,4-dione

Chemical Property:

XLogP3:1.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:276.08585488
Heavy Atom Count:20
Complexity:476

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN1C(=O)C(=C(NC1=O)N(C)C2=CC=CC=C2)[N+](=O)[O-]

Technology Process of 3-methyl-6-(N-methylanilino)-5-nitro-1H-pyrimidine-2,4-dione

There total 1 articles about 3-methyl-6-(N-methylanilino)-5-nitro-1H-pyrimidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58758-67-1
3-methyl-6-(methylphenylamino)-5-nitrouracil

Guidance literature:: 3-Methyl-5-nitro-6-chloruracil, N-Methylanilin;
DOI:10.1248/cpb.25.563

Reference yield:

: 58758-67-1
3-methyl-6-(methylphenylamino)-5-nitrouracil

: 65357-96-2
5-diazo-3-methyl-6-(methylphenylamino)-3H,5H-uracil

Guidance literature:: With hydrogen; sodium nitrite; palladium on activated charcoal; Yield given. Multistep reaction; 1.) water, 2.) 1 h;
DOI:10.1021/ja00352a045

Reference yield:

: 58758-67-1
3-methyl-6-(methylphenylamino)-5-nitrouracil

: 79854-13-0
3-methyl-6-(methylphenylamino)pyrimidine-2,4,5(3H)-trione-5-hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) hydrogen, 2.) sodium nitrite / 1.) palladium/10percent on charcoal / 1.) water, 2.) 1 h

2: 22 percent / triphenyl phosphite / 336 h / Ambient temperature

With triphenyl phosphite; hydrogen; sodium nitrite; palladium on activated charcoal;
DOI:10.1021/ja00352a045