3-methyl-6-(methylphenylamino)-5-(triphenylphosphoranylidenehydrazono)-3H,5H-uracil hydrate

Base Information

Chemical Name:3-methyl-6-(methylphenylamino)-5-(triphenylphosphoranylidenehydrazono)-3H,5H-uracil hydrate
CAS No.:85894-79-7
Molecular Formula:C₃₀H₂₆N₅O₂P
Molecular Weight:519.543
Hs Code.:

Synonyms:3-methyl-6-(methylphenylamino)-5-(triphenylphosphoranylidenehydrazono)-3H,5H-uracil hydrate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methyl-6-(methylphenylamino)-5-(triphenylphosphoranylidenehydrazono)-3H,5H-uracil hydrate

Chemical Property:

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Technology Process of 3-methyl-6-(methylphenylamino)-5-(triphenylphosphoranylidenehydrazono)-3H,5H-uracil hydrate

There total 2 articles about 3-methyl-6-(methylphenylamino)-5-(triphenylphosphoranylidenehydrazono)-3H,5H-uracil hydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.7%

: 603-35-0
triphenylphosphine

: 65357-96-2
5-diazo-3-methyl-6-(methylphenylamino)-3H,5H-uracil

: 85894-79-7
3-methyl-6-(methylphenylamino)-5-(triphenylphosphoranylidenehydrazono)-3H,5H-uracil hydrate

Guidance literature:: In 1,4-dioxane; for 0.5h;
DOI:10.1021/ja00352a045

Reference yield:

: 58758-67-1
3-methyl-6-(methylphenylamino)-5-nitrouracil

: 85894-79-7
3-methyl-6-(methylphenylamino)-5-(triphenylphosphoranylidenehydrazono)-3H,5H-uracil hydrate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) hydrogen, 2.) sodium nitrite / 1.) palladium/10percent on charcoal / 1.) water, 2.) 1 h

2: 82.7 percent / dioxane / 0.5 h

With hydrogen; sodium nitrite; palladium on activated charcoal; In 1,4-dioxane;
DOI:10.1021/ja00352a045