N-(1-Chloro-2-methylprop-1-en-1-yl)-N-methylaniline

Base Information

Chemical Name:N-(1-Chloro-2-methylprop-1-en-1-yl)-N-methylaniline
CAS No.:58933-81-6
Molecular Formula:C11H14ClN
Molecular Weight:195.692
Hs Code.:
DSSTox Substance ID:DTXSID90574841

Synonyms:58933-81-6;N-(1-Chloro-2-methylprop-1-en-1-yl)-N-methylaniline;DTXSID90574841

Suppliers and Price of N-(1-Chloro-2-methylprop-1-en-1-yl)-N-methylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-Chloro-2-methylprop-1-en-1-yl)-N-methylaniline

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:195.0814771
Heavy Atom Count:13
Complexity:188

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=C(N(C)C1=CC=CC=C1)Cl)C

Technology Process of N-(1-Chloro-2-methylprop-1-en-1-yl)-N-methylaniline

There total 4 articles about N-(1-Chloro-2-methylprop-1-en-1-yl)-N-methylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 75755-45-2
N,2-dimethyl-N-phenylpropanethioamide

: 58933-81-6
1-(1-chloro-2-methylprop-1-enyl)-N-methyl-N-phenylamine

Guidance literature:: With phosgene; In dichloromethane; benzene; for 72h; Ambient temperature;
DOI:10.1002/hlca.19830660126

Reference yield:

: 55577-65-6
2,N-dimethyl-N-phenylpropanamide

: 58933-81-6
1-(1-chloro-2-methylprop-1-enyl)-N-methyl-N-phenylamine

Guidance literature:: With triethylamine; N,N-dimethyl-formamide; trichlorophosphate; Yield given. Multistep reaction; 1.) CH₂Cl₂, reflux, 14 h, 2.) CH₂Cl₂, 0 deg C to rt;
DOI:10.1016/S0040-4020(98)00558-4

Reference yield:

: 100-61-8
N-methylaniline

: 58933-81-6
1-(1-chloro-2-methylprop-1-enyl)-N-methyl-N-phenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / CH₂Cl₂ / Ambient temperature

2: 1.) POCl₃, DMF, 2.) DMF, Et₃N / 1.) CH₂Cl₂, reflux, 14 h, 2.) CH₂Cl₂, 0 deg C to rt

With triethylamine; N,N-dimethyl-formamide; trichlorophosphate; In dichloromethane;
DOI:10.1016/S0040-4020(98)00558-4