Phenyl(2-thienyl)methanone phenyl hydrazone

Base Information

Chemical Name:Phenyl(2-thienyl)methanone phenyl hydrazone
CAS No.:7716-31-6
Molecular Formula:C17H14N2S
Molecular Weight:278.378
Hs Code.:
NSC Number:146215
Nikkaji Number:J3.427.657I

Synonyms:MLS002920704;NSC146215;7716-31-6;NSC-146215;Phenyl(2-thienyl)methanone phenyl hydrazone

Suppliers and Price of Phenyl(2-thienyl)methanone phenyl hydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of Phenyl(2-thienyl)methanone phenyl hydrazone

Chemical Property:

Vapor Pressure:1.89E-07mmHg at 25°C
Boiling Point:425.6°Cat760mmHg
Flash Point:211.2°C
Density:1.13g/cm³
XLogP3:4.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:278.08776963
Heavy Atom Count:20
Complexity:317

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=NNC2=CC=CC=C2)C3=CC=CS3
Isomeric SMILES:C1=CC=C(C=C1)/C(=N\NC2=CC=CC=C2)/C3=CC=CS3

Technology Process of Phenyl(2-thienyl)methanone phenyl hydrazone

There total 3 articles about Phenyl(2-thienyl)methanone phenyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 6165-68-0
thiophene boronic acid

: 15424-14-3
N-phenylbenzohydrazonoyl chloride

: 7716-31-6
1-phenyl-2-(phenyl(thiophen-2-yl)methylene)hydrazine

Guidance literature:: With potassium phosphate; In toluene; at 110 ℃; for 16h; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.202001590

Reference yield:

: 588-64-7
benzaldehyde phenylhydrazone

: 7716-31-6
1-phenyl-2-(phenyl(thiophen-2-yl)methylene)hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: N-chloro-succinimide; dimethylsulfide / dichloromethane / 2 h / -78 °C / Inert atmosphere

2: potassium phosphate / toluene / 16 h / 110 °C / Molecular sieve; Inert atmosphere

With potassium phosphate; N-chloro-succinimide; dimethylsulfide; In dichloromethane; toluene;
DOI:10.1002/chem.202001590

Reference yield:

: 100-52-7
benzaldehyde

: 7716-31-6
1-phenyl-2-(phenyl(thiophen-2-yl)methylene)hydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide

2: N-chloro-succinimide; dimethylsulfide / dichloromethane / 2 h / -78 °C / Inert atmosphere

3: potassium phosphate / toluene / 16 h / 110 °C / Molecular sieve; Inert atmosphere

With potassium phosphate; N-chloro-succinimide; dimethylsulfide; sodium hydroxide; In dichloromethane; toluene;
DOI:10.1002/chem.202001590