2-Methyl-2-phenyl-1,2-oxasilinane

Base Information

Chemical Name:2-Methyl-2-phenyl-1,2-oxasilinane
CAS No.:59409-68-6
Molecular Formula:C₁₁H₁₆OSi
Molecular Weight:192.333
Hs Code.:
DSSTox Substance ID:DTXSID00500095

Synonyms:59409-68-6;2-Methyl-2-phenyl-1,2-oxasilinane;SCHEMBL43009;DTXSID00500095

Suppliers and Price of 2-Methyl-2-phenyl-1,2-oxasilinane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Methyl-2-phenyl-1,2-oxasilinane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:192.097041664
Heavy Atom Count:13
Complexity:166

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C[Si]1(CCCCO1)C2=CC=CC=C2

Technology Process of 2-Methyl-2-phenyl-1,2-oxasilinane

There total 8 articles about 2-Methyl-2-phenyl-1,2-oxasilinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 144889-99-6
(2-tetrahydrofuryl)methylphenylsilane

: 59409-68-6
phenyl methyl-siloxane

Guidance literature:: With palladium/alumina; In hexane; for 6h; Ambient temperature;
DOI:10.1016/0022-328X(92)85060-A

Reference yield:

: 130648-88-3
[2-(4,5-dihydrofuryl)]methylphenylsilane

: 59409-68-6
phenyl methyl-siloxane

Guidance literature:: Multi-step reaction with 4 steps

1: 66 percent Chromat_. / NaOH / 0.5 h / Heating

2: 56 percent / H₂ / 5percent Pd/Al₂O₃ / hexane / 6 h / 760 Torr / Ambient temperature

3: 62 percent / LiAlH₄, 18-crown-6 / hexane / 6 h / 60 °C

4: 60 percent / 5percent Pd/Al₂O₃ / hexane / 6 h / Ambient temperature

With sodium hydroxide; palladium/alumina; lithium aluminium tetrahydride; 18-crown-6 ether; hydrogen; palladium/alumina; In hexane;
DOI:10.1016/0022-328X(92)85060-A

Reference yield:

: 144889-92-9
[2-(4,5-dihydrofuryl)]methylphenylmethoxysilane

: 59409-68-6
phenyl methyl-siloxane

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / H₂ / 5percent Pd/Al₂O₃ / hexane / 6 h / 760 Torr / Ambient temperature

2: 62 percent / LiAlH₄, 18-crown-6 / hexane / 6 h / 60 °C

3: 60 percent / 5percent Pd/Al₂O₃ / hexane / 6 h / Ambient temperature

With palladium/alumina; lithium aluminium tetrahydride; 18-crown-6 ether; hydrogen; palladium/alumina; In hexane;
DOI:10.1016/0022-328X(92)85060-A