5-Benzyloxy-2-methylpyridine 1-oxide

Base Information

Chemical Name:5-Benzyloxy-2-methylpyridine 1-oxide
CAS No.:59781-09-8
Molecular Formula:C13H13NO2
Molecular Weight:215.252
Hs Code.:
DSSTox Substance ID:DTXSID80496280
Wikidata:Q82345026

Synonyms:59781-09-8;5-benzyloxy-2-methylpyridine 1-oxide;5-Benzyloxy-2-methyl-pyridine 1-oxide;2-methyl-1-oxido-5-phenylmethoxypyridin-1-ium;Pyridine, 2-methyl-5-(phenylmethoxy)-, 1-oxide;5-benzyloxy-2-methylpyridine N-oxide;5-(benzyloxy)-2-methylpyridine 1-oxide;SCHEMBL228426;DTXSID80496280;FBBMNGYRVLBROF-UHFFFAOYSA-N;MFCD26394830;5-benzyloxy-2-methylpyridine-N-oxide;5-benzyloxy-2-methyl-pyridin-1-oxide;5-benzyloxy-2-methyl-pyridine-1-oxide;5-(benzyloxy)-2-methylpyridine-1-oxide;5-benzyloxy-2-methyl-pyridine-1 -oxide;5-(Benzyloxy)-2-methyl-1-oxo-1lambda~5~-pyridine

Suppliers and Price of 5-Benzyloxy-2-methylpyridine 1-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Benzyloxy-2-methylpyridine 1-oxide

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:215.094628657
Heavy Atom Count:16
Complexity:204

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=[N+](C=C(C=C1)OCC2=CC=CC=C2)[O-]

Technology Process of 5-Benzyloxy-2-methylpyridine 1-oxide

There total 6 articles about 5-Benzyloxy-2-methylpyridine 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 63793-98-6
5-benzyloxy-2-methyl-pyridine

: 59781-09-8
5-(benzyloxy)-2-methylpyridine 1-oxide

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In chloroform; at 20 ℃; for 1h; Cooling with ice;

Reference yield:

: 1121-78-4
5-Hydroxy-2-methylpyridine

: 59781-09-8
5-(benzyloxy)-2-methylpyridine 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / NaH / tetrahydrofuran; dimethylformamide / 20 °C

2: 96 percent / meta-chloroperoxybenzoic acid / CHCl₃ / 1 h / cooling

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(03)00454-1

Reference yield:

: 100-39-0
benzyl bromide

: 59781-09-8
5-(benzyloxy)-2-methylpyridine 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / NaH / tetrahydrofuran; dimethylformamide / 20 °C

2: 96 percent / meta-chloroperoxybenzoic acid / CHCl₃ / 1 h / cooling

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(03)00454-1