1-Cyclopropyl-2-propen-1-one

Base Information

• Chemical Name: 1-Cyclopropyl-2-propen-1-one
• CAS No.: 59819-62-4
• Molecular Formula: C6H8O
• Molecular Weight: 96.12710
• Mol file: 59819-62-4.mol

Synonyms:1-cyclopropyl-propenone;3-Cyclopropyl-1-propen-3-one;cyclopropyl ethenyl ketone;1-cyclopropyl-prop-2-en-1-one;cyclopropyl vinyl ketone;2-Propen-1-one,1-cyclopropyl;1-Cyclopropyl-2-propen-1-one;

Chemical Property of 1-Cyclopropyl-2-propen-1-one

Chemical Property:

• PSA: 17.07000
• LogP: 1.15150

Purity/Quality:

99% ^*data from raw suppliers

1-Cyclopropyl-2-propen-1-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Cyclopropyl-2-propen-1-one

There total 7 articles about 1-Cyclopropyl-2-propen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + Cyclopropyl methyl ketone (765-43-5) → 1-Cyclopropyl-2-propen-1-one (59819-62-4)

Guidance literature:

With N-methylanilinium trifluoroacetate; In tetrahydrofuran; at 20 ℃; Heating / reflux;

Reference yield:

bromo(cyclopropyl)zinc + acryloyl chloride (814-68-6,25189-84-8) → 1-Cyclopropyl-2-propen-1-one (59819-62-4)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 0 ℃;

DOI:10.1021/jm060302x

Reference yield:

Cyclopropyl methyl ketone (765-43-5) + N-methylanilinium trifluoroacetate (29885-95-8) → 1-Cyclopropyl-2-propen-1-one (59819-62-4)

Guidance literature:

In tetrahydrofuran; formaldehyd; diethyl ether;

upstream raw materials:

1-cyclopropyl-3-dimethylamino-1-propanone

methyl iodide

1-trimethylsilyloxy-1,1'-bicyclopropyl

3-chloro-1-cyclopropyl-1-propanone