4,6(1H,5H)-Pyrimidinedione, dihydro-5-[(2-nitrophenyl)methylene]-2-thioxo-

Base Information

• Chemical Name: 4,6(1H,5H)-Pyrimidinedione, dihydro-5-[(2-nitrophenyl)methylene]-2-thioxo-
• CAS No.: 60045-65-0
• Molecular Formula: C11H7N3O4S
• Molecular Weight: 277.26

Synonyms:5-(2-nitro-benzylidene)-2-thioxo-dihydro-pyrimidine-4,6-dione;5-o-Nitrobenzylidene-2-thiobarbituric acid;5-(2-nitro-benzylidene)-2-thio-barbituric acid;5-(2-Nitro-benzyliden)-2-thio-barbitursaeure;

Chemical Property of 4,6(1H,5H)-Pyrimidinedione, dihydro-5-[(2-nitrophenyl)methylene]-2-thioxo-

Chemical Property:

• PSA: 136.11000
• LogP: 1.68990

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,6(1H,5H)-Pyrimidinedione, dihydro-5-[(2-nitrophenyl)methylene]-2-thioxo-

There total 3 articles about 4,6(1H,5H)-Pyrimidinedione, dihydro-5-[(2-nitrophenyl)methylene]-2-thioxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.6%

4,6-dihydroxy-2-mercaptopyrimidine (504-17-6,157796-99-1,924832-30-4) + 2-nitro-benzaldehyde (552-89-6) → 5-[(2'-nitrophenyl)methylidene]-2-thioxodihydropyrimidine-4,6(1H,5H)-dione (60045-65-0)

Guidance literature:

With 1-butyl-3-methylimidazolium Tetrafluoroborate; microwave irradiation;

DOI:10.1080/00397910500288254

Reference yield: 56.0%

→ 5-[(2'-nitrophenyl)methylidene]-2-thioxodihydropyrimidine-4,6(1H,5H)-dione (60045-65-0)

Guidance literature:

In ethanol; water; at 80 ℃; for 2h;

Reference yield:

4,6-dihydroxy-2-mercaptopyrimidine (504-17-6,157796-99-1,924832-30-4) + 2-nitro-benzaldehyde (552-89-6) → C15H9N5O6S2 + 5-[(2'-nitrophenyl)methylidene]-2-thioxodihydropyrimidine-4,6(1H,5H)-dione (60045-65-0)

Guidance literature:

With bromocyane; L-Tartaric acid; In methanol; at 0 - 20 ℃; screw cap tube;

DOI:10.5012/bkcs.2011.32.9.3382

upstream raw materials:

4,6-dihydroxy-2-mercaptopyrimidine

2-nitro-benzaldehyde

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 60045-65-0 4,6(1H,5H)-Pyrimidinedione, dihydro-5-[(2-nitrophenyl)methylene]-2-thioxo-

Send

Send

Metric Ton KG G Pound L ML

Send

Send