2-(cyclohexylideneamino)benzoic Acid

Base Information

Chemical Name:2-(cyclohexylideneamino)benzoic Acid
CAS No.:60054-57-1
Molecular Formula:C13H15NO2
Molecular Weight:217.268
Hs Code.:
DSSTox Substance ID:DTXSID20404925
Nikkaji Number:J1.955.906H

Synonyms:2-(cyclohexylideneamino)benzoic Acid;2-Cyclohexylideneamino-benzoic acid;60054-57-1;cyclohexylideneanthranilic acid;SCHEMBL4956911;DTXSID20404925;WBBFFYZFRHFDIR-UHFFFAOYSA-N

Suppliers and Price of 2-(cyclohexylideneamino)benzoic Acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(cyclohexylideneamino)benzoic Acid

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:217.110278721
Heavy Atom Count:16
Complexity:278

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(=NC2=CC=CC=C2C(=O)O)CC1

Technology Process of 2-(cyclohexylideneamino)benzoic Acid

There total 1 articles about 2-(cyclohexylideneamino)benzoic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 60054-57-1
2-(cyclohexylideneamino)benzoic acid

Guidance literature:: In xylenes; for 18h; Heating / reflux;

Reference yield: 100.0%

: methallylnickel chloride dimer

: 60054-57-1
2-(cyclohexylideneamino)benzoic acid

: 623938-33-0
[2-(cyclohexylideneamino)benzoato-κ(2)N,O](η3-methallyl)nickel(II)

Guidance literature:: With KH; In tetrahydrofuran; acetonitrile; under inert atm. 2-(cyclohexylideneamino)benzoic acid and KH were stirred in THF for 1 h at room temp., MeCN was added and stirred for 30 min, Ni complex was added and stirred for 30 min; solvent was removed in vacuo, residue was extd. with THF, solvent was removed; elem. anal.;
DOI:10.1021/om0303303

Reference yield: 87.0%

: (η3-benzyl)chloro(trimethylphosphine)nickel(II)

: 60054-57-1
2-(cyclohexylideneamino)benzoic acid

: 623938-44-3
[2-(cyclohexylideneamino)benzoato-κ(2)N,O](η1-benzyl)(trimethylphosphine)nickel(II)

Guidance literature:: With KH; In tetrahydrofuran; under inert atm. 2-(cyclohexylideneamino)benzoic acid and KH were stirred in THF overnight at room temp., Ni complex was added and stirred for 1h; solvent was removed under vac., residue was dissolved in toluene, soln. was filtered, solvent was removed, residue was triturated in pentane; elem. anal.;
DOI:10.1021/om0303303