Methyl 4-cyclohexyl-4-oxobut-2-enoate

Base Information

Chemical Name:Methyl 4-cyclohexyl-4-oxobut-2-enoate
CAS No.:60112-28-9
Molecular Formula:C11H16O3
Molecular Weight:196.24300
Hs Code.:2918300090
DSSTox Substance ID:DTXSID70696494
Mol file:60112-28-9.mol

Synonyms:DTXSID70696494;methyl 4-cyclohexyl-4-oxobut-2-enoate;60112-28-9

Suppliers and Price of Methyl 4-cyclohexyl-4-oxobut-2-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Methyl 4-cyclohexyl-4-oxobut-2-enoate

Chemical Property:

PSA：43.37000
LogP:1.86500
XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:196.109944368
Heavy Atom Count:14
Complexity:237

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(=O)C=CC(=O)C1CCCCC1

Technology Process of Methyl 4-cyclohexyl-4-oxobut-2-enoate

There total 5 articles about Methyl 4-cyclohexyl-4-oxobut-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60112-28-9
(E)-methyl 4-oxo-4-cyclohexylbut-2-enoate

Guidance literature:: With thionyl chloride; Erhitzen des hierbei erhaltenen Reaktionsprodukts unter vermindertem Druck;
DOI:10.1021/jo01354a025

Reference yield:

: 2863-48-1
1-cyclohexyl-2-(methylsulfinyl)ethanone

: 96-32-2
bromoacetic acid methyl ester

: 60112-28-9
(E)-methyl 4-oxo-4-cyclohexylbut-2-enoate

Guidance literature:: Multistep reaction; (i) KH, (ii) /BRN= 506256/, (iii) (heating);
DOI:10.1021/ja00427a042

Reference yield:

: 823-76-7
Cyclohexyl methyl ketone

: 60112-28-9
(E)-methyl 4-oxo-4-cyclohexylbut-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: morpholin hydrochloride / 120 °C / Reflux

2: sulfuric acid / Reflux

With sulfuric acid; morpholin hydrochloride;
DOI:10.1039/C6RA24953A