Benzenecarbothioamide, N,2-dimethyl-

Base Information

Chemical Name:Benzenecarbothioamide, N,2-dimethyl-
CAS No.:60253-37-4
Molecular Formula:C9H11NS
Molecular Weight:165.259
Hs Code.:
DSSTox Substance ID:DTXSID00473452
Nikkaji Number:J1.799.087J
Wikidata:Q82302856

Synonyms:Benzenecarbothioamide, N,2-dimethyl-;60253-37-4;SCHEMBL8315307;SCHEMBL23180243;DTXSID00473452

Suppliers and Price of Benzenecarbothioamide, N,2-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Benzenecarbothioamide, N,2-dimethyl-

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:165.06122053
Heavy Atom Count:11
Complexity:145

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1C(=S)NC

Technology Process of Benzenecarbothioamide, N,2-dimethyl-

There total 2 articles about Benzenecarbothioamide, N,2-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 95-46-5
2-methylphenyl bromide

: 556-61-6
methyl thioisocyanate

: 60253-37-4
2,N-dimethylthiobenzamide

Guidance literature:: 2-methylphenyl bromide; With magnesium; In tetrahydrofuran;

methyl thioisocyanate; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1002/1099-0690(200208)2002:15<2573::AID-EJOC2573<3.0.CO;2-S

Reference yield:

: 60253-37-4
2,N-dimethylthiobenzamide

Guidance literature:: aus o-Toluyllithium (aus o-Bromtoluol u. Li-Metall) mit Methylisothiocyanat;
DOI:10.1021/jo00887a023

Reference yield: 91.0%

: 60253-37-4
2,N-dimethylthiobenzamide

: 98-88-4
benzoyl chloride

: N-methyl-N-[(2-methylphenyl)carbonylthioyl]benzamide

Guidance literature:: 2,N-dimethylthiobenzamide; With sec.-butyllithium; In tetrahydrofuran; cyclohexane; at -78 ℃; for 1h;

benzoyl chloride; In tetrahydrofuran; cyclohexane; at -78 ℃; for 0.5h;
DOI:10.1002/1099-0690(200208)2002:15<2573::AID-EJOC2573<3.0.CO;2-S