Methyl 3-amino-5-[[[(dimethylamino)methylene]amino]sulfonyl]-4-phenoxybenzoate

Base Information

Chemical Name:Methyl 3-amino-5-[[[(dimethylamino)methylene]amino]sulfonyl]-4-phenoxybenzoate
CAS No.:60376-74-1
Molecular Formula:C17H19N3O5S
Molecular Weight:377.421
Hs Code.:
European Community (EC) Number:611-968-4
DSSTox Substance ID:DTXSID001137812

Synonyms:SCHEMBL573731;DTXSID001137812;Methyl 3-amino-5-[[[(dimethylamino)methylene]amino]sulfonyl]-4-phenoxybenzoate;60376-74-1

Suppliers and Price of Methyl 3-amino-5-[[[(dimethylamino)methylene]amino]sulfonyl]-4-phenoxybenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Methyl 3-amino-5-[[[(dimethylamino)methylene]amino]sulfonyl]-4-phenoxybenzoate

Chemical Property:

Vapor Pressure:7.17E-12mmHg at 25°C
XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:7
Exact Mass:377.10454189
Heavy Atom Count:26
Complexity:596

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C=NS(=O)(=O)C1=CC(=CC(=C1OC2=CC=CC=C2)N)C(=O)OC

Technology Process of Methyl 3-amino-5-[[[(dimethylamino)methylene]amino]sulfonyl]-4-phenoxybenzoate

There total 5 articles about Methyl 3-amino-5-[[[(dimethylamino)methylene]amino]sulfonyl]-4-phenoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28328-53-2
3-nitro-4-phenoxy-5-sulfamoylbenzoic acid

: 60376-74-1
5-amino-3-(dimethylaminomethylenesulfamoyl)-4-phenoxybenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 50 °C

2: acetonitrile / 20 °C

3: water; ammonium chloride; iron / ethanol / 1.05 h / 85 °C

With thionyl chloride; water; iron; ammonium chloride; In ethanol; acetonitrile;

Reference yield:

: 108-95-2,27073-41-2
phenol

: 60376-74-1
5-amino-3-(dimethylaminomethylenesulfamoyl)-4-phenoxybenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / water / 85 °C

1.2: 20 °C

2.1: thionyl chloride / 50 °C

3.1: acetonitrile / 20 °C

4.1: water; ammonium chloride; iron / ethanol / 1.05 h / 85 °C

With thionyl chloride; water; iron; sodium hydrogencarbonate; ammonium chloride; In ethanol; water; acetonitrile;

Reference yield:

: 22892-96-2
4-chloro-3-nitro-5-sulfamoylbenzoic acid

: 60376-74-1
5-amino-3-(dimethylaminomethylenesulfamoyl)-4-phenoxybenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate / water / 85 °C

1.2: 20 °C

2.1: thionyl chloride / 50 °C

3.1: acetonitrile / 20 °C

4.1: water; ammonium chloride; iron / ethanol / 1.05 h / 85 °C

With thionyl chloride; water; iron; sodium hydrogencarbonate; ammonium chloride; In ethanol; water; acetonitrile;