1H-Pyrrole, 2,2'-(1,4-cyclohexanediyl)bis[1-butyl-

Base Information

Chemical Name:1H-Pyrrole, 2,2'-(1,4-cyclohexanediyl)bis[1-butyl-
CAS No.:60550-21-2
Molecular Formula:C₂₂H₃₄N₂
Molecular Weight:326.525
Hs Code.:
DSSTox Substance ID:DTXSID60482666

Synonyms:1H-Pyrrole, 2,2'-(1,4-cyclohexanediyl)bis[1-butyl-;60550-21-2;DTXSID60482666

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Pyrrole, 2,2'-(1,4-cyclohexanediyl)bis[1-butyl-

Chemical Property:

XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:8
Exact Mass:326.272199093
Heavy Atom Count:24
Complexity:314

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCN1C=CC=C1C2CCC(CC2)C3=CC=CN3CCCC

Technology Process of 1H-Pyrrole, 2,2'-(1,4-cyclohexanediyl)bis[1-butyl-

There total 3 articles about 1H-Pyrrole, 2,2'-(1,4-cyclohexanediyl)bis[1-butyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 133406-74-3
3,4-Dichloro-1-[4-(3,4-dichloro-butyryl)-cyclohexyl]-butan-1-one

: 109-73-9,85404-21-3
N-butylamine

: 60550-21-2
1,1'-dibutyl-2,2'-cyclohexane-1,4-diyl-bis-pyrrole

Guidance literature:: In diethyl ether; for 4h; Heating;
DOI:10.1007/BF00484356

Reference yield:

: 13170-66-6,14571-47-2,19988-54-6
trans-1,4-cyclohexanedicarboxylic acid chloride

: 60550-21-2
1,1'-dibutyl-2,2'-cyclohexane-1,4-diyl-bis-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: AlCl₃ / 1,2-dichloro-ethane / -20 °C

2: 57 percent / diethyl ether / 4 h / Heating

With aluminium trichloride; In diethyl ether; 1,2-dichloro-ethane;
DOI:10.1007/BF00484356

Reference yield:

: 60550-21-2
1,1'-dibutyl-2,2'-cyclohexane-1,4-diyl-bis-pyrrole

Guidance literature:: Dichlorid von Hexahydro-terephthalsaeure, 1) AlCl3/Dichloraethan (-20-25gradC), 2) Allylchlorid (20gradC; 2 Std.), 3) Eis, HCl - Extraktion, 4) Umloesen in Ae., n-Butylamin (-10gradC) - Erhitzen (1 Std., nach 1 Tag);

upstream raw materials:

3,4-Dichloro-1-[4-(3,4-dichloro-butyryl)-cyclohexyl]-butan-1-one

N-butylamine

trans-1,4-cyclohexanedicarboxylic acid chloride

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