2,5-Dibromo-N,N-dimethylaniline

Base Information

• Chemical Name: 2,5-Dibromo-N,N-dimethylaniline
• CAS No.: 60573-63-9
• Molecular Formula: C8H9Br2N
• Molecular Weight: 278.974
• DSSTox Substance ID: DTXSID00489932
• Wikidata: Q82333483

Synonyms:2,5-Dibromo-N,N-dimethylaniline;60573-63-9;SCHEMBL9485990;DTXSID00489932

Chemical Property of 2,5-Dibromo-N,N-dimethylaniline

Chemical Property:

• XLogP3: 3.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 278.90813
• Heavy Atom Count: 11
• Complexity: 127

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=C(C=CC(=C1)Br)Br

Technology Process of 2,5-Dibromo-N,N-dimethylaniline

There total 3 articles about 2,5-Dibromo-N,N-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2,5-dibromoaniline (3638-73-1) + methyl iodide (74-88-4) → 2,5-dibromo-N,N-dimethylaniline (60573-63-9)

Guidance literature:

With potassium carbonate; at 20 - 100 ℃; for 48h; Inert atmosphere;

DOI:10.1021/jo500661u

Reference yield:

2,5-dibromoaniline (3638-73-1) + dimethyl sulfate (77-78-1) → 2,5-dibromo-N,N-dimethylaniline (60573-63-9)

Guidance literature:

With sodium carbonate;

Reference yield:

→ 2,5-dibromo-N,N-dimethylaniline (60573-63-9)

Guidance literature:

2-Brom-N.N-dimethylanilin (3), Dibromisocyanursaeure (1) (Bromierung);

upstream raw materials:

2,5-dibromoaniline

dimethyl sulfate

methyl iodide

Downstream raw materials:

4-Brom-2-(N_.N-dimethylamino)phenyldiphenylcarbinol

2,5-dicyano-N,N-dimethylaniline

N,N-dimethyl-2,5-bis[(trimethylsilyl)ethynyl]aniline

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