1,2-Dibromotetradecane

Base Information

• Chemical Name: 1,2-Dibromotetradecane
• CAS No.: 6064-45-5
• Molecular Formula: C14H28Br2
• Molecular Weight: 356.184
• DSSTox Substance ID: DTXSID80399065
• Nikkaji Number: J2.695.316B
• Mol file: 6064-45-5.mol

Synonyms:1,2-dibromotetradecane;6064-45-5;DTXSID80399065;AKOS024390865

Chemical Property of 1,2-Dibromotetradecane

Chemical Property:

• XLogP3: 7.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 12
• Exact Mass: 356.05373
• Heavy Atom Count: 16
• Complexity: 126

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCCC(CBr)Br

Technology Process of 1,2-Dibromotetradecane

There total 2 articles about 1,2-Dibromotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-tetradecyl-N'-tosylhydrazine (52756-06-6) → 1-Bromotetradecane (112-71-0) + 1,2-dibromotetradecane (6064-45-5) + toluene-p-sulfonyl bromide (1950-69-2)

Guidance literature:

With bromine; In chloroform; for 2.5h; Ambient temperature;

DOI:10.1016/S0040-4020(01)88628-2

Reference yield:

1-tetradecene (1120-36-1) → 1,2-dibromotetradecane (6064-45-5) + 1,2-dichlor-tetradecan (701920-83-4) + 1-chlor-2-brom-tetradecan + 1-brom-2-chlor-tetradecan

Guidance literature:

With bromine; chlorine; In dichloromethane; at -40 ℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

Reference yield:

1,2-dibromotetradecane (6064-45-5) → 1-tetradecyne (765-10-6)

Guidance literature:

With sodium amide; In dimethyl sulfoxide; at 65 - 70 ℃; for 9h;

DOI:10.1016/S0040-4020(01)92790-5

upstream raw materials:

N-tetradecyl-N'-tosylhydrazine

1-tetradecene

Downstream raw materials:

1-tetradecyne

2-tetradecyne